N-bis(trimethylsilyl)methyl-N-(2-phenylpropyl)-2-diazo-3-oxobutanamide

Base Information

Chemical Name:N-bis(trimethylsilyl)methyl-N-(2-phenylpropyl)-2-diazo-3-oxobutanamide
CAS No.:951289-49-9
Molecular Formula:C₂₀H₃₃N₃O₂Si₂
Molecular Weight:403.672
Hs Code.:

Synonyms:N-bis(trimethylsilyl)methyl-N-(2-phenylpropyl)-2-diazo-3-oxobutanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-bis(trimethylsilyl)methyl-N-(2-phenylpropyl)-2-diazo-3-oxobutanamide

Chemical Property:

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Technology Process of N-bis(trimethylsilyl)methyl-N-(2-phenylpropyl)-2-diazo-3-oxobutanamide

There total 6 articles about N-bis(trimethylsilyl)methyl-N-(2-phenylpropyl)-2-diazo-3-oxobutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134340-00-4
bis(trimethylsilyl)methylamine

: 951289-49-9
N-bis(trimethylsilyl)methyl-N-(2-phenylpropyl)-2-diazo-3-oxobutanamide

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether

2: NaBH₄ / methanol / 20 °C

3: DMAP / tetrahydrofuran

4: methanesulfonyl azide; DBU / acetonitrile

With dmap; sodium tetrahydroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; Methanesulfonyl azide; In tetrahydrofuran; methanol; diethyl ether; acetonitrile;
DOI:10.1021/jo051042e

Reference yield:

: N-(bis-trimethylsilanyl-methyl)-3-oxo-N-(2-phenyl-propyl)-butyramide

: 951289-49-9
N-bis(trimethylsilyl)methyl-N-(2-phenylpropyl)-2-diazo-3-oxobutanamide

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; Methanesulfonyl azide; In acetonitrile;
DOI:10.1021/jo051042e

Reference yield:

: 951289-26-2
(bis-trimethylsilanyl-methyl)-(2-phenyl-propyl)-amine

: 951289-49-9
N-bis(trimethylsilyl)methyl-N-(2-phenylpropyl)-2-diazo-3-oxobutanamide

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / tetrahydrofuran

2: methanesulfonyl azide; DBU / acetonitrile

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; Methanesulfonyl azide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo051042e