SASSOLITE

Base Information

• Chemical Name: SASSOLITE
• CAS No.: 14635-83-7
• Molecular Formula: BH₃O₃
• Molecular Weight: 61.833
• Mol file: 14635-83-7.mol

Synonyms:Sassolite(7CI,8CI)

Chemical Property of SASSOLITE

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of SASSOLITE

There total 714 articles about SASSOLITE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

boron tribromide (10294-33-4) → boron + boron trioxide + boron nitride (10043-11-5) + boron + boric acid (11113-50-1,14635-83-7)

Guidance literature:

With H₂; N₂; In neat (no solvent); Electric Arc; pulse heating (plasma, puls repitition rate 5-12,5 Hz, N2 flow 0.2 - 1.65 l/min, H2 flow 1.13 - 3.5 l/min9; further products; X-ray diffraction;

Reference yield:

phosphorus(V) chloride * 2 BBr3 → hydrogenchloride (7647-01-0,15364-23-5) + phosphoric acid (86119-84-8,7664-38-2) + hydrogen bromide (10035-10-6,12258-64-9) + boric acid (11113-50-1,14635-83-7)

Guidance literature:

With moist air; In neat (no solvent); hydrolysis with moist air under formation of H3PO4, H3BO3 and evolution of HCl and HBr;;

Reference yield:

boron trioxide → boric acid (11113-50-1,14635-83-7) + metaboric acid (13460-50-9)

Guidance literature:

With nitric acid; HNO3 conc. between 60-94%;

upstream raw materials:

5-bromo-2-chloropyridine

pyrographite

triacetoxyborane

dihydrogen peroxide

Downstream raw materials:

Anilinium-bis-{o-phenylendioxo}-borat^(1-)

(OC(C₆H₅)CHC(CH₃)O)2B⁽¹⁺⁾*HSO₄^(1-)={(OC(C₆H₅)CHC(CH₃)O)2B}HSO₄

1:1 adduct of boric acid and triphenylphosphine oxide

(HO)2BNH-2-CH₃C₆H₄

Refernces

• 1、 Wang, Yi,Shen, Jialu,Huang, Yu,Liu, Xiang,Zhao, Qiuxia,Astruc, Didier. "Acid- and Base-Catalyzed Hydrolytic Hydrogen Evolution from Diboronic Acid". . p. 3013 - 3018. Retrieved 2021/03/26.
• 2、 Feng, Gang,Huang, Meiling,Lu, Zhang-Hui,Yao, Qilu,Zou, Hongtao. "Nickel-Ceria Nanowires Embedded in Microporous Silica: Controllable Synthesis, Formation Mechanism, and Catalytic Applications". supporting information. p. 5781 - 5790. Retrieved 2020/04/20.