3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-1-(tert-butyl-dimethyl-silanyloxy)-6,6-dimethyl-cyclohex-2-enecarbonitrile

Base Information

Chemical Name:3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-1-(tert-butyl-dimethyl-silanyloxy)-6,6-dimethyl-cyclohex-2-enecarbonitrile
CAS No.:1020202-77-0
Molecular Formula:C₂₅H₃₄N₄OSi
Molecular Weight:434.657
Hs Code.:

Synonyms:3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-1-(tert-butyl-dimethyl-silanyloxy)-6,6-dimethyl-cyclohex-2-enecarbonitrile

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Chemical Property of 3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-1-(tert-butyl-dimethyl-silanyloxy)-6,6-dimethyl-cyclohex-2-enecarbonitrile

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Technology Process of 3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-1-(tert-butyl-dimethyl-silanyloxy)-6,6-dimethyl-cyclohex-2-enecarbonitrile

There total 1 articles about 3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-1-(tert-butyl-dimethyl-silanyloxy)-6,6-dimethyl-cyclohex-2-enecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1020202-97-4
acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester

: 75-16-1
methylmagnesium bromide

: 1020202-77-0
3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-1-(tert-butyl-dimethyl-silanyloxy)-6,6-dimethyl-cyclohex-2-enecarbonitrile

Guidance literature:: methylmagnesium bromide; With copper(l) iodide; lithium bromide; In tetrahydrofuran; diethyl ether; for 0.5h; Cooling with ice;

acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester; In tetrahydrofuran; diethyl ether; for 0.5h; Cooling with ice;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether; Cooling with ice;
DOI:10.1021/ol800429j