Technology Process of C33H36O8
There total 4 articles about C33H36O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 9h;
DOI:10.1021/ma501164u
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C
2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 20 °C
3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 9 h / 0 - 20 °C
With
dmap; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine;
In
tetrahydrofuran; dichloromethane;
3: |Mitsunobu Displacement;
DOI:10.1021/ma501164u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 20 °C
2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 9 h / 0 - 20 °C
With
di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; triphenylphosphine;
In
tetrahydrofuran;
2: |Mitsunobu Displacement;
DOI:10.1021/ma501164u