6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-2-N-phenoxyacetyl-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxy-6-thioguanosine

Base Information

Chemical Name:6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-2-N-phenoxyacetyl-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxy-6-thioguanosine
CAS No.:1242460-54-3
Molecular Formula:C₄₁H₆₇N₅O₇SSi₂
Molecular Weight:830.249
Hs Code.:

Synonyms:6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-2-N-phenoxyacetyl-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxy-6-thioguanosine

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Chemical Property of 6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-2-N-phenoxyacetyl-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxy-6-thioguanosine

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Technology Process of 6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-2-N-phenoxyacetyl-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxy-6-thioguanosine

There total 1 articles about 6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-2-N-phenoxyacetyl-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxy-6-thioguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1225490-73-2
6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxy-6-thioguanosine

: 701-99-5
Phenoxyacetyl chloride

: 1242460-54-3
6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-2-N-phenoxyacetyl-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxy-6-thioguanosine

Guidance literature:: 6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-3',5'-O-bis(tert-butyldimethylsilyl)-2'-deoxy-6-thioguanosine; With pyridine; benzotriazol-1-ol; In acetonitrile; at 20 ℃; for 1.5h; Molecular sieve;

Phenoxyacetyl chloride; In acetonitrile; for 8.5h;
DOI:10.1080/15257770903155576