N-[(S)-2-chloropropionyl]-N-p-methoxybenzyl-L-Tyr(2,6-dichlorobenzyl)-OMe

Base Information

Chemical Name:N-[(S)-2-chloropropionyl]-N-p-methoxybenzyl-L-Tyr(2,6-dichlorobenzyl)-OMe
CAS No.:1342305-95-6
Molecular Formula:C₂₈H₂₈Cl₃NO₅
Molecular Weight:564.893
Hs Code.:

Synonyms:N-[(S)-2-chloropropionyl]-N-p-methoxybenzyl-L-Tyr(2,6-dichlorobenzyl)-OMe

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Chemical Property of N-[(S)-2-chloropropionyl]-N-p-methoxybenzyl-L-Tyr(2,6-dichlorobenzyl)-OMe

Chemical Property:

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Technology Process of N-[(S)-2-chloropropionyl]-N-p-methoxybenzyl-L-Tyr(2,6-dichlorobenzyl)-OMe

There total 3 articles about N-[(S)-2-chloropropionyl]-N-p-methoxybenzyl-L-Tyr(2,6-dichlorobenzyl)-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 29617-66-1
(S)-2-chloropropanoic acid

: 610314-16-4
(S)-3-[4-(2,6-Dichloro-benzyloxy)-phenyl]-2-(4-methoxy-benzylamino)-propionic acid methyl ester

: 1342305-95-6
N-[(S)-2-chloropropionyl]-N-p-methoxybenzyl-L-Tyr(2,6-dichlorobenzyl)-OMe

Guidance literature:: (S)-2-chloropropanoic acid; With trichloroacetonitrile; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

(S)-3-[4-(2,6-Dichloro-benzyloxy)-phenyl]-2-(4-methoxy-benzylamino)-propionic acid methyl ester; With methyloxirane; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2011.08.025

Reference yield:

: (S)-O-(2,6-dichlorobenzyl)tyrosine methyl ester

: 1342305-95-6
N-[(S)-2-chloropropionyl]-N-p-methoxybenzyl-L-Tyr(2,6-dichlorobenzyl)-OMe

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / methanol / 1.5 h / 20 °C

1.2: 0.5 h / 0 - 20 °C

2.1: trichloroacetonitrile; triphenylphosphine / tetrahydrofuran / 1 h / 0 - 20 °C

With triethylamine; trichloroacetonitrile; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1016/j.ejmech.2011.08.025

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1342305-95-6
N-[(S)-2-chloropropionyl]-N-p-methoxybenzyl-L-Tyr(2,6-dichlorobenzyl)-OMe

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / methanol / 1.5 h / 20 °C

1.2: 0.5 h / 0 - 20 °C

2.1: trichloroacetonitrile; triphenylphosphine / tetrahydrofuran / 1 h / 0 - 20 °C

With triethylamine; trichloroacetonitrile; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1016/j.ejmech.2011.08.025