4,4'-<1-Bis(2-chlorethyl)aminomethyl-2-ethylethylen>bis-(phenol)-hydrochlorid

Base Information

Chemical Name:4,4'-<1-Bis(2-chlorethyl)aminomethyl-2-ethylethylen>bis-(phenol)-hydrochlorid
CAS No.:85628-80-4
Molecular Formula:C₂₁H₂₇Cl₂NO₂*ClH
Molecular Weight:432.818
Hs Code.:

Synonyms:4,4'-<1-Bis(2-chlorethyl)aminomethyl-2-ethylethylen>bis-(phenol)-hydrochlorid

Suppliers and Price of 4,4'-<1-Bis(2-chlorethyl)aminomethyl-2-ethylethylen>bis-(phenol)-hydrochlorid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-<1-Bis(2-chlorethyl)aminomethyl-2-ethylethylen>bis-(phenol)-hydrochlorid

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Technology Process of 4,4'-<1-Bis(2-chlorethyl)aminomethyl-2-ethylethylen>bis-(phenol)-hydrochlorid

There total 5 articles about 4,4'-<1-Bis(2-chlorethyl)aminomethyl-2-ethylethylen>bis-(phenol)-hydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 85628-79-1
2,2'-imino>diethanol

: 85628-80-4
4,4'-<1-Bis(2-chlorethyl)aminomethyl-2-ethylethylen>bis-(phenol)-hydrochlorid

Guidance literature:: With thionyl chloride; In 1,4-dioxane; 1.) 45 deg C, 2 h, 2.) room temp., 12 h;
DOI:10.1002/ardp.19833160316

Reference yield:

: 79568-15-3
2,3-Bis(4-methoxyphenyl)valeronitril

: 85628-80-4
4,4'-<1-Bis(2-chlorethyl)aminomethyl-2-ethylethylen>bis-(phenol)-hydrochlorid

Guidance literature:: Multi-step reaction with 4 steps

1: H₂, 37percent aq. HCl / 10percent Pd/C / ethanol / Ambient temperature

2: 56 percent / ethanol / 120 h / Ambient temperature

3: 72 percent / BBr₃ / CH₂Cl₂ / 1.) 5 deg C, 2 h, 2.) room temp., 12 h

4: 62 percent / SOCl₂ / dioxane / 1.) 45 deg C, 2 h, 2.) room temp., 12 h

With hydrogenchloride; thionyl chloride; hydrogen; boron tribromide; palladium on activated charcoal; In 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1002/ardp.19833160316

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 85628-80-4
4,4'-<1-Bis(2-chlorethyl)aminomethyl-2-ethylethylen>bis-(phenol)-hydrochlorid

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / C₂H₅ONa / ethanol / 5 h / Ambient temperature

2: 1.) Mg / 1.) ether, 2.) THF, reflux, 1 h; room temp., 20 h

3: H₂, 37percent aq. HCl / 10percent Pd/C / ethanol / Ambient temperature

4: 56 percent / ethanol / 120 h / Ambient temperature

5: 72 percent / BBr₃ / CH₂Cl₂ / 1.) 5 deg C, 2 h, 2.) room temp., 12 h

6: 62 percent / SOCl₂ / dioxane / 1.) 45 deg C, 2 h, 2.) room temp., 12 h

With hydrogenchloride; thionyl chloride; hydrogen; sodium ethanolate; boron tribromide; magnesium; palladium on activated charcoal; In 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1002/ardp.19833160316