5-Bromo-N-methyl-3-nitropyridin-2-amine

Base Information

• Chemical Name: 5-Bromo-N-methyl-3-nitropyridin-2-amine
• CAS No.: 70232-59-6
• Molecular Formula: C₆H₆BrN₃O₂
• Molecular Weight: 232.037
• Hs Code.: 2933399990
• DSSTox Substance ID: DTXSID10446490
• Mol file: 70232-59-6.mol

Synonyms:5-Bromo-N-methyl-3-nitropyridin-2-amine;70232-59-6;5-Bromo-2-methylamino-3-nitropyridine;5-Bromo-2-(methylamino)-3-nitropyridine;2-Pyridinamine, 5-bromo-N-methyl-3-nitro-;(5-Bromo-3-nitro-pyridin-2-yl)-methyl-amine;MFCD07375006;SCHEMBL790395;DTXSID10446490;KOPIJZGJPUGTHU-UHFFFAOYSA-N;AC6653;AKOS010477139;AB40930;AS-64298;SY129382;CS-0096376;FT-0678603;EN300-205605;5-Bromo-N-methyl-3-nitropyridin-2-amine, AldrichCPR;Z784892682

Chemical Property of 5-Bromo-N-methyl-3-nitropyridin-2-amine

Chemical Property:

• Storage Temp.: 2-8°C
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 230.96434
• Heavy Atom Count: 12
• Complexity: 173

Purity/Quality:

99%, ^*data from raw suppliers

5-Bromo-N-methyl-3-nitropyridin-2-amine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNC1=C(C=C(C=N1)Br)[N+](=O)[O-]

Technology Process of 5-Bromo-N-methyl-3-nitropyridin-2-amine

There total 2 articles about 5-Bromo-N-methyl-3-nitropyridin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

5-bromo-2-chloro-3-nitropyridine (67443-38-3) + methylamine (74-89-5) → 5-bromo-N-methyl-3-nitropyridin-2-amine (70232-59-6)

Guidance literature:

In tetrahydrofuran; at 0 ℃; for 0.5h;

Reference yield: 83.0%

5-bromo-2-chloro-3-nitropyridine (67443-38-3) → 5-bromo-N-methyl-3-nitropyridin-2-amine (70232-59-6)

Guidance literature:

With methylamine; In isopropyl alcohol;

Reference yield: 100.0%

5-bromo-N-methyl-3-nitropyridin-2-amine (70232-59-6) → 5-bromo-N2-methylpyridine-2,3-diamine (89415-54-3)

Guidance literature:

5-bromo-N-methyl-3-nitropyridin-2-amine; With iron; acetic acid; In water; at 20 ℃; for 0.666667h;

With sodium hydroxide; water;

upstream raw materials:

5-bromo-2-chloro-3-nitropyridine

methylamine

Downstream raw materials:

N-methyl-3-nitro-5-phenylpyridin-2-amine

5-bromo-N²-methylpyridine-2,3-diamine

N-[5-bromo-2-(methylamino)-3-pyridinyl]benzenesulfonamide

C₁₈H₂₄BN₃O₄S

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