3-N-benzyloxycarbonylaminopropyl 2,3-di-O-acetyl-4-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:3-N-benzyloxycarbonylaminopropyl 2,3-di-O-acetyl-4-O-benzyl-α-L-rhamnopyranoside
CAS No.:132799-05-4
Molecular Formula:C₂₈H₃₅NO₉
Molecular Weight:529.587
Hs Code.:

Synonyms:3-N-benzyloxycarbonylaminopropyl 2,3-di-O-acetyl-4-O-benzyl-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-N-benzyloxycarbonylaminopropyl 2,3-di-O-acetyl-4-O-benzyl-α-L-rhamnopyranoside

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Technology Process of 3-N-benzyloxycarbonylaminopropyl 2,3-di-O-acetyl-4-O-benzyl-α-L-rhamnopyranoside

There total 1 articles about 3-N-benzyloxycarbonylaminopropyl 2,3-di-O-acetyl-4-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: ethyl 2,3-di-O-acetyl-4-O-benzyl-1-thio-α-L-rhamnopyranoside

: 132799-05-4
3-N-benzyloxycarbonylaminopropyl 2,3-di-O-acetyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With 4 A molecular sieve; methyl trifluoromethanesulfonate; In dichloromethane; for 18h; Ambient temperature;
DOI:10.1016/S0008-6215(97)10013-1

Reference yield:

: 132799-05-4
3-N-benzyloxycarbonylaminopropyl 2,3-di-O-acetyl-4-O-benzyl-α-L-rhamnopyranoside

: 132799-06-5
[3-((2R,3R,4S,5R,6S)-5-Benzyloxy-3,4-dihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-propyl]-carbamic acid benzyl ester

Guidance literature:: With sodium methylate; In methanol; for 2h;
DOI:10.1016/S0008-6215(97)10013-1

Reference yield:

: 132799-05-4
3-N-benzyloxycarbonylaminopropyl 2,3-di-O-acetyl-4-O-benzyl-α-L-rhamnopyranoside

: 212199-01-4
Acetic acid (2R,3R,4R,5R,6S)-5-benzyloxy-2-(3-benzyloxycarbonylamino-propoxy)-4-hydroxy-6-methyl-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaOMe / methanol / 2 h

2: p-TsOH / toluene; CH₂Cl₂ / 0.5 h

3: H₂O, p-TsOH / toluene; CH₂Cl₂ / 0.33 h

With water; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane; toluene;
DOI:10.1016/S0008-6215(97)10013-1