1-[4-(Dimethyl-phenyl-silanyl)-phenyl]-1,1,2,2-tetramethyl-2-phenyl-disilane

Base Information

• Chemical Name: 1-[4-(Dimethyl-phenyl-silanyl)-phenyl]-1,1,2,2-tetramethyl-2-phenyl-disilane
• CAS No.: 144752-32-9
• Molecular Formula: C₂₄H₃₂Si₃
• Molecular Weight: 404.775

Synonyms:1-[4-(Dimethyl-phenyl-silanyl)-phenyl]-1,1,2,2-tetramethyl-2-phenyl-disilane

Chemical Property of 1-[4-(Dimethyl-phenyl-silanyl)-phenyl]-1,1,2,2-tetramethyl-2-phenyl-disilane

Chemical Property:

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Technology Process of 1-[4-(Dimethyl-phenyl-silanyl)-phenyl]-1,1,2,2-tetramethyl-2-phenyl-disilane

There total 3 articles about 1-[4-(Dimethyl-phenyl-silanyl)-phenyl]-1,1,2,2-tetramethyl-2-phenyl-disilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-bis(2-phenyltetramethyldisilanyl)benzene (144752-29-4) + isobutene (115-11-7,15220-85-6) → Dimethylphenylsilane (766-77-8) + 1-(4-Dimethylsilanyl-phenyl)-1,1,2,2-tetramethyl-2-phenyl-disilane (144752-33-0) + 1-[4-(Dimethyl-phenyl-silanyl)-phenyl]-1,1,2,2-tetramethyl-2-phenyl-disilane (144752-32-9) + 4-(isobutyldimethylsilyl)-3-(phenyldimethylsilyl)-1-(2-phenyltetramethyldisilanyl)benzene (144752-30-7) + 2-(isobutyldimethylsilyl)-1-silyl>benzene (144752-31-8) + 1,4-bis(isobutyldimethylsilyl)-2,5-bis(phenyldimethylsilyl)benzene (144772-54-3)

Guidance literature:

In benzene; for 0.583333h; Product distribution; Irradiation; other solvents;

DOI:10.1016/0022-328X(92)83395-X

Reference yield:

1-chloro-2-phenyltetramethyldisilane (941-15-1) + (4-bromophenyl)dimethylphenyl-1-ylsilane (18407-37-9) → 1-[4-(Dimethyl-phenyl-silanyl)-phenyl]-1,1,2,2-tetramethyl-2-phenyl-disilane (144752-32-9)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1.) THF, 2.) THF, reflux, 43 h;

DOI:10.1016/0022-328X(92)83395-X

Reference yield:

1,4-bis(2-phenyltetramethyldisilanyl)benzene (144752-29-4) + isobutene (115-11-7,15220-85-6) → 1-[4-(Dimethyl-phenyl-silanyl)-phenyl]-1,1,2,2-tetramethyl-2-phenyl-disilane (144752-32-9) + 4-(isobutyldimethylsilyl)-3-(phenyldimethylsilyl)-1-(2-phenyltetramethyldisilanyl)benzene (144752-30-7) + 2-(isobutyldimethylsilyl)-1-silyl>benzene (144752-31-8) + 1,4-bis(isobutyldimethylsilyl)-2,5-bis(phenyldimethylsilyl)benzene (144772-54-3)

Guidance literature:

In benzene; for 0.583333h; Further byproducts given; Irradiation;

DOI:10.1016/0022-328X(92)83395-X

upstream raw materials:

1-chloro-2-phenyltetramethyldisilane

(4-bromophenyl)dimethylphenyl-1-ylsilane

1,4-bis(2-phenyltetramethyldisilanyl)benzene

isobutene

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