benzyl methyl trithiocarbonate

Base Information

Chemical Name:benzyl methyl trithiocarbonate
CAS No.:82843-64-9
Molecular Formula:C₉H₁₀S₃
Molecular Weight:214.376
Hs Code.:

Synonyms:benzyl methyl trithiocarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl methyl trithiocarbonate

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Technology Process of benzyl methyl trithiocarbonate

There total 6 articles about benzyl methyl trithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 75-15-0,12122-00-8
carbon disulfide

: 100-53-8
phenylmethanethiol

: 74-88-4
methyl iodide

: 82843-64-9
benzyl methyl trithiocarbonate

Guidance literature:: phenylmethanethiol; With triethylamine; at 25 ℃; for 0.25h; Neat (no solvent);

carbon disulfide; In water; at 25 ℃; for 0.5h;

methyl iodide; In water; at 25 ℃; for 1h; in air atmosphere;
DOI:10.1007/s00706-008-0864-x

Reference yield: 76.0%

: 74-88-4
methyl iodide

: 82843-64-9
benzyl methyl trithiocarbonate

Guidance literature:: With carbon disulfide; In chloroform;
DOI:10.1002/ejic.200500948

Reference yield: 76.0%

: 933445-78-4
(1,4,8,12-tetraazacyclopentadecane)zinc(II) benzyltrithiocarbonate perchlorate

: 74-88-4
methyl iodide

: (1,4,8,12-tetraazacyclopentadecane)zinc(II) iodide perchlorate

: 82843-64-9
benzyl methyl trithiocarbonate

Guidance literature:: In chloroform; byproducts: benzyl methyl sulfide; CS2 added to Zn complex in CHCl3, reacted for 30 min, treated with CH3I,stirred overnight; evapd., washed (pentane), concd., chromy.(silica - pentane), elem. anal., NMR;
DOI:10.1002/ejic.200500948