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Technology Process of CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)(1+)*PF6(1-)=[CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)]PF6

CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)(1+)*PF6(1-)=[CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)]PF6

Base Information
  • Chemical Name:CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)(1+)*PF6(1-)=[CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)]PF6
  • CAS No.:292146-98-6
  • Molecular Formula:C17H20N2OPPd*F6P
  • Molecular Weight:550.717
  • Hs Code.:
CH<sub>3</sub>CN(CH<sub>3</sub>)Pd((C<sub>6</sub>H<sub>5</sub>)2PNHC(O)CH<sub>3</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[CH<sub>3</sub>CN(CH<sub>3</sub>)Pd((C<sub>6</sub>H<sub>5</sub>)2PNHC(O)CH<sub>3</sub>)]PF<sub>6</sub>

Synonyms:CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)(1+)*PF6(1-)=[CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)]PF6

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Chemical Property of CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)(1+)*PF6(1-)=[CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)]PF6
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Technology Process of CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)(1+)*PF6(1-)=[CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)]PF6

There total 2 articles about CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)(1+)*PF6(1-)=[CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

thallium(I) hexafluorophosphate
60969-19-9

thallium(I) hexafluorophosphate

chloromethyl(1,5-cyclooctadiene)palladium(II)

chloromethyl(1,5-cyclooctadiene)palladium(II)

acetonitrile
75-05-8,26809-02-9

acetonitrile

N-(diphenylphosphino)acetamide

N-(diphenylphosphino)acetamide

CH<sub>3</sub>CN(CH<sub>3</sub>)Pd((C<sub>6</sub>H<sub>5</sub>)2PNHC(O)CH<sub>3</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[CH<sub>3</sub>CN(CH<sub>3</sub>)Pd((C<sub>6</sub>H<sub>5</sub>)2PNHC(O)CH<sub>3</sub>)]PF<sub>6</sub>
292146-98-6

CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)(1+)*PF6(1-)=[CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)]PF6

Guidance literature:
In acetonitrile; inert atm.; stirred for 30 min; filtered, solvent evapd, ppt. washed (diethyl ether), dried (vac.); elem. anal.;
DOI:10.1002/1521-3773(20000818)39:16<2867::AID-ANIE2867>3.0.CO;2-X

Reference yield: 90.0%

thallium(I) hexafluorophosphate
60969-19-9

thallium(I) hexafluorophosphate

[PdCl(Me)(1,5-cyclodiene)]
63936-85-6

[PdCl(Me)(1,5-cyclodiene)]

acetonitrile
75-05-8,26809-02-9

acetonitrile

Pd(CH<sub>3</sub>)P(C<sub>6</sub>H<sub>5</sub>)2NHCOCH<sub>3</sub>(NCCH<sub>3</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=Pd(CH<sub>3</sub>)P(C<sub>6</sub>H<sub>5</sub>)2NHCOCH<sub>3</sub>(NCCH<sub>3</sub>)(PF<sub>6</sub>)
292146-98-6

Pd(CH3)P(C6H5)2NHCOCH3(NCCH3)(1+)*PF6(1-)=Pd(CH3)P(C6H5)2NHCOCH3(NCCH3)(PF6)

Guidance literature:
In acetonitrile; CH3CN, ambient temp., stirring for 30 min then TlPF6 was added and stirred for 30 min (N2 atm.); filtered, evapd., ppt. was washed with Et2O and dried in vac.; elem. anal.;
DOI:10.1039/b002386h

Reference yield: 88.0%

CH<sub>3</sub>CN(CH<sub>3</sub>)Pd((C<sub>6</sub>H<sub>5</sub>)2PNHC(O)CH<sub>3</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[CH<sub>3</sub>CN(CH<sub>3</sub>)Pd((C<sub>6</sub>H<sub>5</sub>)2PNHC(O)CH<sub>3</sub>)]PF<sub>6</sub>
292146-98-6

CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)(1+)*PF6(1-)=[CH3CN(CH3)Pd((C6H5)2PNHC(O)CH3)]PF6

carbon monoxide
201230-82-2

carbon monoxide

PdCOCH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2NHCOCH<sub>3</sub>(NCCH<sub>3</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=PdCOCH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2NHCOCH<sub>3</sub>NCCH<sub>3</sub>(PF<sub>6</sub>)
292146-87-3

PdCOCH3P(C6H5)2NHCOCH3(NCCH3)(1+)*PF6(1-)=PdCOCH3P(C6H5)2NHCOCH3NCCH3(PF6)

Guidance literature:
In dichloromethane; CO bubbled at room temp. for 1 h; filtered, volatiles removed (vac.), ppt. washed (pentane), dried (vac.); elem. anal.;
DOI:10.1002/1521-3773(20000818)39:16<2867::AID-ANIE2867>3.0.CO;2-X
upstream raw materials:

thallium(I) hexafluorophosphate

[PdCl(Me)(1,5-cyclodiene)]

acetonitrile

Downstream raw materials:

Pd(CH3)(P(C6H5)2N(CH3)COCH3)2(1+)*PF6(1-)=Pd(CH3)(P(C6H5)2N(CH3)COCH3)2(PF6)

PdCH3P(C6H5)2NHCOCH3P(C6H5)2NHCOCH3(1+)*PF6(1-)=PdCH3P(C6H5)2NHCOCH3P(C6H5)2NHCOCH3(PF6)

Pd(CH3)(P(C6H5)2N(CH3)COCH3)(P(C6H5)2NHCOCH3)(1+)*PF6(1-)=Pd(CH3)(P(C6H5)2N(CH3)COCH3)(P(C6H5)2NHCOCH3)(PF6)

PdCOCH3P(C6H5)2NHCOCH3(NCCH3)(1+)*PF6(1-)=PdCOCH3P(C6H5)2NHCOCH3NCCH3(PF6)

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