4-(4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzyl methyl ether

Base Information

• Chemical Name: 4-(4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzyl methyl ether
• CAS No.: 944476-09-9
• Molecular Formula: C₁₇H₂₁NO
• Molecular Weight: 255.36
• Mol file: 944476-09-9.mol

Synonyms:4-(4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzyl methyl ether

Chemical Property of 4-(4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzyl methyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzyl methyl ether

There total 3 articles about 4-(4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methanol (67-56-1) → 4-(4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)benzyl methyl ether (944476-09-9)

Guidance literature:

With sodium hydroxide; In chloroform; at 20 ℃; for 20h;

DOI:10.1002/mrc.1830

Reference yield: 99.0%

methanol (67-56-1) + 4-(4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)benzyl acetate (944476-07-7) → 4-(4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)benzyl methyl ether (944476-09-9)

Guidance literature:

With aluminum oxide; at 20 ℃; for 20h;

DOI:10.1016/j.tet.2007.02.094

Reference yield:

4-(4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl)benzyl alcohol → 4-(4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)benzyl methyl ether (944476-09-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / triethylamine / CH₂Cl₂ / 2 h / 20 °C

2: 99 percent / neutral alumina / 20 h / 20 °C

With aluminum oxide; triethylamine; In dichloromethane;

DOI:10.1016/j.tet.2007.02.094

upstream raw materials:

methanol

4-(4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzyl acetate