Boc-N-Me-Dl-Val-Oh

Base Information

Chemical Name:Boc-N-Me-Dl-Val-Oh
CAS No.:13850-91-4
Molecular Formula:C₁₁H₂₁NO₄
Molecular Weight:231.292
Hs Code.:2922509090
DSSTox Substance ID:DTXSID00398479
Mol file:13850-91-4.mol

Synonyms:Boc-N-Me-Dl-Val-Oh;13850-91-4;Boc-L-N-Me-Val-OH;3-methyl-2-[methyl-[(2-methylpropan-2-yl)oxycarbonyl]amino]butanoic Acid;DL-Valine, N-[(1,1-dimethylethoxy)carbonyl]-N-methyl-;2-{[(tert-butoxy)carbonyl](methyl)amino}-3-methylbutanoic acid;N-Boc-N-methylvaline;Boc-N-Me-D-Val-OH;Boc-N-methyl-DL-valine;MFCD00038760;Q301;Boc-DL-Me-Val-OH;SCHEMBL67120;Valine,N-[(1,1-dimethylethoxy)carbonyl]-N-methyl-;DTXSID00398479;MFCD00153317;STK042657;AKOS005383401;CS-W006587;DS-2322;HY-W006587;N-(tert-butoxycarbonyl)-N-methylvaline;SY057266;FT-0629968;FT-0688521;EN300-3222157;A886222;N-Methyl-N-{[(2-methyl-2-propanyl)oxy]carbonyl}valine;2-(tert-butoxycarbonyl(methyl)amino)-3-methylbutanoic acid

Suppliers and Price of Boc-N-Me-Dl-Val-Oh

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
Boc-N-methyl-DL-valine
500mg
$ 333.00

TRC
Boc-N-Me-DL-Val-OH
50mg
$ 60.00

Matrix Scientific
Boc-N-Me-DL-Val-OH >95%
10g
$ 684.00

Matrix Scientific
Boc-N-Me-DL-Val-OH >95%
1g
$ 90.00

Matrix Scientific
Boc-N-Me-DL-Val-OH >95%
5g
$ 396.00

Crysdot
Boc-N-Me-DL-Val-OH 95+%
25g
$ 485.00

chempep
Boc-N-Me-DL-Val-OH
5g
$ 300.00

chempep
Boc-N-Me-DL-Val-OH
25g
$ 910.00

Chem-Impex
Boc--methyl-DL-valine ≥ 98%
25G
$ 790.00

Chem-Impex
Boc--methyl-DL-valine ≥ 98%
5G
$ 230.00

Total 28 raw suppliers

Chemical Property of Boc-N-Me-Dl-Val-Oh

Chemical Property:

Vapor Pressure:5.74E-05mmHg at 25°C
Refractive Index:1.466
Boiling Point:322.4oC at 760 mmHg
Flash Point:148.8oC
PSA：66.84000
Density:1.069g/cm3
LogP:1.96250
Storage Temp.:Store at RT.
XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:231.14705815
Heavy Atom Count:16
Complexity:268

Purity/Quality:

97% ^*data from raw suppliers

Boc-N-methyl-DL-valine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C(C(=O)O)N(C)C(=O)OC(C)(C)C

Technology Process of Boc-N-Me-Dl-Val-Oh

There total 6 articles about Boc-N-Me-Dl-Val-Oh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 22838-58-0
Boc-D-Val-OH

: 74-88-4
methyl iodide

: 13850-91-4,45170-31-8,89536-85-6
(R)-2-(tert-butoxycarbonyl(methyl)amino)-3-methylbutanoic acid

Guidance literature:: Boc-D-Val-OH; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1039/c5ob02505b

Reference yield:

: 640-68-6,25609-85-2,7004-03-7,921-10-8
D-Val-OH

: 24424-99-5
di-tert-butyl dicarbonate

: 74-88-4
methyl iodide

: 13850-91-4,45170-31-8,89536-85-6
(R)-2-(tert-butoxycarbonyl(methyl)amino)-3-methylbutanoic acid

Guidance literature:: D-Val-OH; di-tert-butyl dicarbonate; With sodium hydroxide; In 1,4-dioxane;

methyl iodide; In tetrahydrofuran;
DOI:10.1021/ol0478786