N-benzyloxycarbonyl-L-phenylalanyl-DL-α-(ethylthio)glycine methyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-L-phenylalanyl-DL-α-(ethylthio)glycine methyl ester
CAS No.:188302-22-9
Molecular Formula:C₂₂H₂₆N₂O₅S
Molecular Weight:430.525
Hs Code.:

Synonyms:N-benzyloxycarbonyl-L-phenylalanyl-DL-α-(ethylthio)glycine methyl ester

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Chemical Property of N-benzyloxycarbonyl-L-phenylalanyl-DL-α-(ethylthio)glycine methyl ester

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Technology Process of N-benzyloxycarbonyl-L-phenylalanyl-DL-α-(ethylthio)glycine methyl ester

There total 3 articles about N-benzyloxycarbonyl-L-phenylalanyl-DL-α-(ethylthio)glycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 872130-35-3
N-benzyloxycarbonyl-L-phenylalanyl-DL-α-acetoxyglycine methyl ester

: 75-08-1
ethanethiol

: 188302-22-9
N-benzyloxycarbonyl-L-phenylalanyl-DL-α-(ethylthio)glycine methyl ester

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In tetrahydrofuran; 1) 2 h, -78 deg C 2) to r.t., overnight;
DOI:10.1016/S0040-4039(00)79711-5

Reference yield:

: 17554-22-2
N-benzyloxycarbonyl-L-phenylalanyl-L-threonine methyl ester

: 188302-22-9
N-benzyloxycarbonyl-L-phenylalanyl-DL-α-(ethylthio)glycine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 4 Angstroem molecular sieve / ethyl acetate / 2 h / Heating

2: 75 percent / Et₃N / CH₂Cl₂ / 15 h / Ambient temperature

With 4 A molecular sieve; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(01)88040-6

Reference yield:

: 23828-09-3
N-(benzyloxycarbonyl)-L-phenylalanyl-L-serine methyl ester

: 188302-22-9
N-benzyloxycarbonyl-L-phenylalanyl-DL-α-(ethylthio)glycine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / molecular sieve 4A / ethyl acetate / Heating

2: 90 percent / diazabicyclo<2.2.2>octane / tetrahydrofuran / 1) 2 h, -78 deg C 2) to r.t., overnight

With 1,4-diaza-bicyclo[2.2.2]octane; 4 A molecular sieve; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/S0040-4039(00)79711-5