4(e)-(2,5-bis-benzyloxy-3,4-dicyano-phenyl)-cyclohexane-(a)-carbaldehyde

Base Information

Chemical Name:4(e)-(2,5-bis-benzyloxy-3,4-dicyano-phenyl)-cyclohexane-(a)-carbaldehyde
CAS No.:179617-87-9
Molecular Formula:C₂₉H₂₆N₂O₃
Molecular Weight:450.537
Hs Code.:

Synonyms:4(e)-(2,5-bis-benzyloxy-3,4-dicyano-phenyl)-cyclohexane-(a)-carbaldehyde

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Chemical Property of 4(e)-(2,5-bis-benzyloxy-3,4-dicyano-phenyl)-cyclohexane-(a)-carbaldehyde

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Technology Process of 4(e)-(2,5-bis-benzyloxy-3,4-dicyano-phenyl)-cyclohexane-(a)-carbaldehyde

There total 4 articles about 4(e)-(2,5-bis-benzyloxy-3,4-dicyano-phenyl)-cyclohexane-(a)-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 179617-85-7
4-(2,5-Bis-benzyloxy-3,4-dicyano-phenyl)-cyclohexanecarboxylic acid methyl ester

: 179617-87-9
4(e)-(2,5-bis-benzyloxy-3,4-dicyano-phenyl)-cyclohexane-(a)-carbaldehyde

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; dichloromethane; at -95 ℃; for 1h;
DOI:10.1016/0040-4020(96)00405-X

Reference yield:

: 100-39-0
benzyl bromide

: 179617-87-9
4(e)-(2,5-bis-benzyloxy-3,4-dicyano-phenyl)-cyclohexane-(a)-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / K₂CO₃ / acetone / 1 h / Heating

2: 94 percent / diisobutylaluminium hydride / diethyl ether; CH₂Cl₂ / 1 h / -95 °C

With diisobutylaluminium hydride; potassium carbonate; In diethyl ether; dichloromethane; acetone;
DOI:10.1016/0040-4020(96)00405-X

Reference yield:

: 2-<4-(Methoxycarbonyl)cyclohexyl>-p-benzochinon

: 179617-87-9
4(e)-(2,5-bis-benzyloxy-3,4-dicyano-phenyl)-cyclohexane-(a)-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 98percent H₂SO₄ / propan-2-ol; H₂O / 10 h / 20 - 30 °C

2: 97 percent / K₂CO₃ / acetone / 1 h / Heating

3: 94 percent / diisobutylaluminium hydride / diethyl ether; CH₂Cl₂ / 1 h / -95 °C

With sulfuric acid; diisobutylaluminium hydride; potassium carbonate; In diethyl ether; dichloromethane; water; isopropyl alcohol; acetone;
DOI:10.1016/0040-4020(96)00405-X