(R)-(-)-2,4-dimethoxy-6-trifluoromethylsulfonyloxybenzoic acid (1-methyl-hept-7-enyl)ester

Base Information

Chemical Name:(R)-(-)-2,4-dimethoxy-6-trifluoromethylsulfonyloxybenzoic acid (1-methyl-hept-7-enyl)ester
CAS No.:183384-63-6
Molecular Formula:C₁₈H₂₃F₃O₇S
Molecular Weight:440.438
Hs Code.:

Synonyms:(R)-(-)-2,4-dimethoxy-6-trifluoromethylsulfonyloxybenzoic acid (1-methyl-hept-7-enyl)ester

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Chemical Property of (R)-(-)-2,4-dimethoxy-6-trifluoromethylsulfonyloxybenzoic acid (1-methyl-hept-7-enyl)ester

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Technology Process of (R)-(-)-2,4-dimethoxy-6-trifluoromethylsulfonyloxybenzoic acid (1-methyl-hept-7-enyl)ester

There total 7 articles about (R)-(-)-2,4-dimethoxy-6-trifluoromethylsulfonyloxybenzoic acid (1-methyl-hept-7-enyl)ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 183384-57-8
(R)-(-)-4,6-dimethoxy-2-hydroxybenzoic acid (1-methyl-hept-7-enyl)ester

: 183384-63-6
(R)-(-)-2,4-dimethoxy-6-trifluoromethylsulfonyloxybenzoic acid (1-methyl-hept-7-enyl)ester

Guidance literature:: With pyridine; 0 deg C -> RT;
DOI:10.1016/0040-4039(96)01590-0

Reference yield:

: 3187-19-7
2,4-dimethoxysalicylic acid

: 183384-63-6
(R)-(-)-2,4-dimethoxy-6-trifluoromethylsulfonyloxybenzoic acid (1-methyl-hept-7-enyl)ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / EtOOC-N=N-COOEt; PPh₃ / diethyl ether / 25 °C

2: 91 percent / pyridine / 0 - 25 °C

With pyridine; triphenylphosphine; diethylazodicarboxylate; In diethyl ether; 1: Esterification / 2: Esterification;
DOI:10.1016/S0040-4020(99)00302-6

Reference yield:

: 129234-94-2
(S)-2-hydroxy-7-octene

: 183384-63-6
(R)-(-)-2,4-dimethoxy-6-trifluoromethylsulfonyloxybenzoic acid (1-methyl-hept-7-enyl)ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / EtOOC-N=N-COOEt; PPh₃ / diethyl ether / 25 °C

2: 91 percent / pyridine / 0 - 25 °C

With pyridine; triphenylphosphine; diethylazodicarboxylate; In diethyl ether; 1: Esterification / 2: Esterification;
DOI:10.1016/S0040-4020(99)00302-6