(S)-tert-butyl(2-(3-(tert-butyldimethylsilyloxy)phenoxy)propoxy)dimethylsilane

Base Information

Chemical Name:(S)-tert-butyl(2-(3-(tert-butyldimethylsilyloxy)phenoxy)propoxy)dimethylsilane
CAS No.:1352571-27-7
Molecular Formula:C₂₁H₄₀O₃Si₂
Molecular Weight:396.718
Hs Code.:

Synonyms:(S)-tert-butyl(2-(3-(tert-butyldimethylsilyloxy)phenoxy)propoxy)dimethylsilane

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Chemical Property of (S)-tert-butyl(2-(3-(tert-butyldimethylsilyloxy)phenoxy)propoxy)dimethylsilane

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Technology Process of (S)-tert-butyl(2-(3-(tert-butyldimethylsilyloxy)phenoxy)propoxy)dimethylsilane

There total 3 articles about (S)-tert-butyl(2-(3-(tert-butyldimethylsilyloxy)phenoxy)propoxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1352571-26-6
(S)-3-(1-hydroxypropan-2-yloxy)phenol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1352571-27-7
(S)-tert-butyl(2-(3-(tert-butyldimethylsilyloxy)phenoxy)propoxy)dimethylsilane

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 0.75h;

Reference yield:

: 136-36-7
benzoate d'hydroxy-3 phenyle

: 1352571-27-7
(S)-tert-butyl(2-(3-(tert-butyldimethylsilyloxy)phenoxy)propoxy)dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / -20 - 20 °C

2.2: 1 h / 0 °C / Reflux

3.1: 1H-imidazole / dichloromethane / 0.75 h / 0 - 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; dichloromethane; 1.1: Mitsunobu reaction;

Reference yield:

: 1352571-25-5
(S)-3-(1-methoxy-1-oxopropan-2-yloxy)phenyl benzoate

: 1352571-27-7
(S)-tert-butyl(2-(3-(tert-butyldimethylsilyloxy)phenoxy)propoxy)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / -20 - 20 °C

1.2: 1 h / 0 °C / Reflux

2.1: 1H-imidazole / dichloromethane / 0.75 h / 0 - 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;