Technology Process of C31H31N5O2
There total 12 articles about C31H31N5O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos;
In
1,4-dioxane;
at 100 ℃;
for 2h;
Inert atmosphere;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C
2: triethylamine; copper diacetate / pyridine / 24 h / 25 - 30 °C
3: sodium t-butanolate; XPhos; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 2 h / 100 °C / Inert atmosphere; Microwave irradiation
With
tris-(dibenzylideneacetone)dipalladium(0); copper diacetate; potassium carbonate; triethylamine; sodium t-butanolate; XPhos;
In
1,4-dioxane; pyridine; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -78 °C
2: manganese(IV) oxide / tetrahydrofuran / 5 h / 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C
4: triethylamine; copper diacetate / pyridine / 24 h / 25 - 30 °C
5: sodium t-butanolate; XPhos; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 2 h / 100 °C / Inert atmosphere; Microwave irradiation
With
manganese(IV) oxide; tris-(dibenzylideneacetone)dipalladium(0); lithium aluminium tetrahydride; copper diacetate; potassium carbonate; triethylamine; sodium t-butanolate; XPhos;
In
tetrahydrofuran; 1,4-dioxane; pyridine; N,N-dimethyl-formamide;