4'-(p-methylphenyl)-2,2':6',2''-terpyridine platinum(II) chloride

Base Information

Chemical Name:4'-(p-methylphenyl)-2,2':6',2''-terpyridine platinum(II) chloride
CAS No.:152385-99-4
Molecular Formula:C₂₂H₁₇ClN₃Pt*ClO₄
Molecular Weight:653.381
Hs Code.:

Synonyms:4'-(p-methylphenyl)-2,2':6',2''-terpyridine platinum(II) chloride

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Chemical Property of 4'-(p-methylphenyl)-2,2':6',2''-terpyridine platinum(II) chloride

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Technology Process of 4'-(p-methylphenyl)-2,2':6',2''-terpyridine platinum(II) chloride

There total 1 articles about 4'-(p-methylphenyl)-2,2':6',2''-terpyridine platinum(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10025-99-7
potassium tetrachloroplatinate(II)

: sodium perchlorate

: 89972-77-0
4'-(4-methylphenyl)-2,2':6',2-terpyridine

: 152385-99-4
4'-(p-methylphenyl)-2,2':6',2''-terpyridine platinum(II) chloride

Guidance literature:: In water; acetonitrile; refluxing mixture of terpyridine and Pt complex in water-acetonitrile (1/1 v/v) for 24h; filtration of the resulting hot suspension into a soln. of NaClO4 in water, pptn.; filtration; washing with water and ethanol; recrystn. by diffusing diethyl ether into a acetonitrile-HCON(CH3)2 soln.; elem. anal.;
DOI:10.1039/DT9930002933

Reference yield: 81.0%

: 152385-99-4
4'-(p-methylphenyl)-2,2':6',2''-terpyridine platinum(II) chloride

: 1202800-89-2
N-(3-(triethoxysilyl)propyl)-4-ethynylbenzamide

: ((C₁₂H₉N(C₅H₄N)2)Pt(CCC₆H₄CONHC₃H₆Si(OC₂H₅)3))⁽¹⁺⁾*ClO₄^(1-)*H₂O=((C₁₂H₉N(C₅H₄N)2)Pt(CCC₆H₄CONHC₃H₆Si(OC₂H₅)3))ClO₄*H₂O

Guidance literature:: With sodium perchlorate; triethylamine; copper(l) iodide; In triethylamine; N,N-dimethyl-formamide; Sonication; (N2) mixt. Pt complex and ethynylbenzamide,DMF and Et3N was stirred for 15 min, CuI was added and ultrasonicated for 8 h, NaClO4 was added and ultrasonicated for 1 h; ether was added, ppt. was filtered, rinsed with water and ether, dissolved in MeCN, ether was added, ppt. was filtered and dried; elem. anal.;
DOI:10.1039/b916488j