S-(+)-2-[4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]-2-(4-chlorophenyl)ethanoic acid methyl ester

Base Information

Chemical Name:S-(+)-2-[4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]-2-(4-chlorophenyl)ethanoic acid methyl ester
CAS No.:1220286-47-4
Molecular Formula:C₂₂H₂₅Cl₂N₅O₄
Molecular Weight:494.378
Hs Code.:

Synonyms:S-(+)-2-[4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]-2-(4-chlorophenyl)ethanoic acid methyl ester

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Chemical Property of S-(+)-2-[4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]-2-(4-chlorophenyl)ethanoic acid methyl ester

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Technology Process of S-(+)-2-[4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]-2-(4-chlorophenyl)ethanoic acid methyl ester

There total 3 articles about S-(+)-2-[4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]-2-(4-chlorophenyl)ethanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.1%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1081766-09-7,59410-89-8
(S)-4-chlorophenylglycine methyl ester hydrochloride

: 150824-47-8
nitenpiram

: 1220286-47-4
S-(+)-2-[4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]-2-(4-chlorophenyl)ethanoic acid methyl ester

Guidance literature:: With triethylamine; In ethanol; at 60 - 75 ℃; Microwave irradiation;
DOI:10.1021/jf904397k

Reference yield:

: (E)-N-(6-chloro-3-pyridylmethyl)-N-ethyl-1-chloro-2-nitroethylene-1-amine

: 1220286-47-4
S-(+)-2-[4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]-2-(4-chlorophenyl)ethanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 3 - 7 °C

2: triethylamine / ethanol / 60 - 75 °C / Microwave irradiation

With triethylamine; In ethanol;
DOI:10.1021/jf904397k

Reference yield:

: 120739-77-7
N-(6-chloro-pyridin-3-yl)methyl-N-ethylamine

: 1220286-47-4
S-(+)-2-[4-[[(6-chloro-3-pyridinyl)methyl]ethylamino]-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]-2-(4-chlorophenyl)ethanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: chloroform / 2 - 7 °C

2: 3 - 7 °C

3: triethylamine / ethanol / 60 - 75 °C / Microwave irradiation

With triethylamine; In ethanol; chloroform;
DOI:10.1021/jf904397k