triisopropyl-[3,5-dimethyl-4-(4'-methoxymethoxy-3'-vinylbenzyl)phenoxy]silane

Base Information

Chemical Name:triisopropyl-[3,5-dimethyl-4-(4'-methoxymethoxy-3'-vinylbenzyl)phenoxy]silane
CAS No.:852949-77-0
Molecular Formula:C₂₈H₄₂O₃Si
Molecular Weight:454.725
Hs Code.:

Synonyms:triisopropyl-[3,5-dimethyl-4-(4'-methoxymethoxy-3'-vinylbenzyl)phenoxy]silane

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Chemical Property of triisopropyl-[3,5-dimethyl-4-(4'-methoxymethoxy-3'-vinylbenzyl)phenoxy]silane

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Technology Process of triisopropyl-[3,5-dimethyl-4-(4'-methoxymethoxy-3'-vinylbenzyl)phenoxy]silane

There total 7 articles about triisopropyl-[3,5-dimethyl-4-(4'-methoxymethoxy-3'-vinylbenzyl)phenoxy]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 852949-19-0
5-(2,6-dimethyl-4-triisopropylsilanyloxybenzyl)-2-methoxymethoxy-benzaldehyde

: 1779-49-3
Methyltriphenylphosphonium bromide

: 852949-77-0
triisopropyl-[3,5-dimethyl-4-(4'-methoxymethoxy-3'-vinylbenzyl)phenoxy]silane

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 1h;

5-(2,6-dimethyl-4-triisopropylsilanyloxybenzyl)-2-methoxymethoxy-benzaldehyde; In tetrahydrofuran; hexane; at 20 ℃; for 2.5h;

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 852949-77-0
triisopropyl-[3,5-dimethyl-4-(4'-methoxymethoxy-3'-vinylbenzyl)phenoxy]silane

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / dichloromethane / 2.67 h / 10 - 20 °C

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

2.2: 1 h / -78 °C

3.1: hydrogen / palladium on activated charcoal / acetic acid; ethyl acetate / 5 h / 20 °C / 760.05 Torr

4.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; diethyl ether / 1 h / -20 - 0 °C

4.2: 2 h / 0 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

5.2: 2.5 h / 20 °C

With 1H-imidazole; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; acetic acid; ethyl acetate;

Reference yield:

: 852949-17-8
(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol

: 852949-77-0
triisopropyl-[3,5-dimethyl-4-(4'-methoxymethoxy-3'-vinylbenzyl)phenoxy]silane

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium on activated charcoal / acetic acid; ethyl acetate / 5 h / 20 °C / 760.05 Torr

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; diethyl ether / 1 h / -20 - 0 °C

2.2: 2 h / 0 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

3.2: 2.5 h / 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; hexane; acetic acid; ethyl acetate;