N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide
CAS No.:1416164-19-6
Molecular Formula:C₁₆H₁₇FN₂O₃S
Molecular Weight:336.387
Hs Code.:

Synonyms:N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Suppliers and Price of N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

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Technology Process of N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

There total 1 articles about N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 455-91-4
1-(3-fluoro-4-methoxyphenyl)ethanone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1416164-19-6
N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: In ethanol; for 6h; Reflux;
DOI:10.1002/cmdc.201500069

Reference yield: 72.0%

: 496-15-1
1-indoline

: 637-87-6
1-Chloro-4-iodobenzene

: 1416164-19-6
N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

: 1416164-70-9
1-(4-(1-(3-fluoro-4-methoxyphenyl)vinyl)phenyl)indoline

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); sodium t-butanolate; XPhos; In fluorobenzene; at 120 ℃; for 6h; Sealed tube;
DOI:10.1021/ol303194s

Reference yield: 61.0%

: 1416164-19-6
N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

: (Z)-ethyl N-(5-bromo-2-chlorophenyl)acetimidate

: 104-94-9
4-methoxy-aniline

: 5-[1-(3-fluoro-4-methoxyphenyl)vinyl]-1-(4-methoxyphenyl)-2-methyl-1H-benzo[d]imidazole

Guidance literature:: N’-(1-(3-fluoro-4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide; (Z)-ethyl N-(5-bromo-2-chlorophenyl)acetimidate; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; lithium tert-butoxide; DavePhos; In 1,4-dioxane; at 100 ℃; for 1.5h; Inert atmosphere; Sealed tube;

4-methoxy-aniline; With lithium tert-butoxide; at 130 ℃; for 3h; Sealed tube;
DOI:10.1002/adsc.201600173