methyl 3-(N-allyl-N-benzylamino)-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)propanoate

Base Information

Chemical Name:methyl 3-(N-allyl-N-benzylamino)-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)propanoate
CAS No.:1206614-44-9
Molecular Formula:C₂₃H₃₆N₂O₃
Molecular Weight:388.55
Hs Code.:

Synonyms:methyl 3-(N-allyl-N-benzylamino)-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)propanoate

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Chemical Property of methyl 3-(N-allyl-N-benzylamino)-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)propanoate

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Technology Process of methyl 3-(N-allyl-N-benzylamino)-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)propanoate

There total 1 articles about methyl 3-(N-allyl-N-benzylamino)-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 473914-75-9
3-(allyl-benzyl-amino)-propionic acid methyl ester

: 1206614-44-9
methyl 3-(N-allyl-N-benzylamino)-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)propanoate

: methyl 1-benzyl-4-[(2,2,6,6-tetramethylpiperidin-1-yloxy)methyl]pyrrolidine-3-carboxylate

: methyl 1-benzyl-4-[(2,2,6,6-tetramethylpiperidin-1-yloxy)methyl]pyrrolidine-3-carboxylate

Guidance literature:: 3-(allyl-benzyl-amino)-propionic acid methyl ester; With lithium diisopropyl amide; In 1,2-dimethoxyethane; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; With ferrocenium hexafluorophosphate; In 1,2-dimethoxyethane; hexane; at -78 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.10.034