coahuilensol, methyl ether

Base Information

Chemical Name:coahuilensol, methyl ether
CAS No.:72473-09-7
Molecular Formula:C₁₀H₁₂O
Molecular Weight:148.205
Hs Code.:

Synonyms:coahuilensol, methyl ether

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Chemical Property of coahuilensol, methyl ether

Chemical Property:

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Technology Process of coahuilensol, methyl ether

There total 4 articles about coahuilensol, methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 54884-55-8
2-methoxy-6-methyl-benzaldehyde

: 1779-49-3
Methyltriphenylphosphonium bromide

: 72473-09-7
coahuilensol, methyl ether

Guidance literature:: Methyltriphenylphosphonium bromide; With t-PeOK; In tetrahydrofuran; toluene; at 20 ℃; for 0.25h; Inert atmosphere;

2-methoxy-6-methyl-benzaldehyde; In tetrahydrofuran; toluene; at 20 ℃; for 0.75h; Cooling with ice;
DOI:10.1002/chem.201501959

Reference yield:

: 2944-49-2
2,3-dimethylanisole

: 72473-09-7
coahuilensol, methyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(ll) sulfate pentahydrate; dipotassium peroxodisulfate / acetonitrile / 0.95 - 20 °C

2.1: t-PeOK / tetrahydrofuran; toluene / 0.25 h / 20 °C / Inert atmosphere

2.2: 0.75 h / 20 °C / Cooling with ice

With dipotassium peroxodisulfate; copper(ll) sulfate pentahydrate; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1002/chem.201501959

Reference yield:

: 526-75-0
2,3-Dimethylphenol

: 72473-09-7
coahuilensol, methyl ether

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 45 °C

2.1: copper(ll) sulfate pentahydrate; dipotassium peroxodisulfate / acetonitrile / 0.95 - 20 °C

3.1: t-PeOK / tetrahydrofuran; toluene / 0.25 h / 20 °C / Inert atmosphere

3.2: 0.75 h / 20 °C / Cooling with ice

With dipotassium peroxodisulfate; copper(ll) sulfate pentahydrate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/chem.201501959