closo-1,2-dicarbahexaborane

Base Information

• Chemical Name: closo-1,2-dicarbahexaborane
• CAS No.: 20693-68-9
• Molecular Formula: C₂H₆B₄
• Molecular Weight: 73.3136

Synonyms:closo-1,2-dicarbahexaborane

Chemical Property of closo-1,2-dicarbahexaborane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of closo-1,2-dicarbahexaborane

There total 2 articles about closo-1,2-dicarbahexaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

2,3-dicarba-nido-hexaborane(8) (18972-20-8) → closo-1,2-dicarbahexaborane (20693-68-9) + trimethylborane (593-90-8)

Guidance literature:

palladium; dehydrogenisation with Pd, 75-130°C;

Reference yield:

2,3-dicarba-nido-hexaborane(8) (18972-20-8) + monosilane (7440-21-3) → pentaborane(9) (19624-22-7) + closo-1,2-dicarbahexaborane (20693-68-9) + 1,5-dicarba-closo-pentaborane (20693-66-7) + 1,6-dicarba-closo-hexaborane(6) (20693-67-8) + diborane (19287-45-7)

Guidance literature:

In gaseous matrix; 3 kV, in ozone apparatus, contains methyl silane;

DOI:10.1016/S0022-328X(00)81572-7

upstream raw materials:

2,3-dicarba-nido-hexaborane⁽⁸⁾

monosilane

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