N,N,N'-tris[(6-bromo-2,2'-bipyridine-5'-yl)methyl]-N'-p-nitrobenzylethylenediamine

Base Information

Chemical Name:N,N,N'-tris[(6-bromo-2,2'-bipyridine-5'-yl)methyl]-N'-p-nitrobenzylethylenediamine
CAS No.:474363-03-6
Molecular Formula:C₄₂H₃₄Br₃N₉O₂
Molecular Weight:936.503
Hs Code.:

Synonyms:N,N,N'-tris[(6-bromo-2,2'-bipyridine-5'-yl)methyl]-N'-p-nitrobenzylethylenediamine

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Chemical Property of N,N,N'-tris[(6-bromo-2,2'-bipyridine-5'-yl)methyl]-N'-p-nitrobenzylethylenediamine

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Technology Process of N,N,N'-tris[(6-bromo-2,2'-bipyridine-5'-yl)methyl]-N'-p-nitrobenzylethylenediamine

There total 2 articles about N,N,N'-tris[(6-bromo-2,2'-bipyridine-5'-yl)methyl]-N'-p-nitrobenzylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 102494-88-2
N-(p-nitrobenzyl)ethylenediamine

: 334001-82-0
6-bromo-5'-bromomethyl-2,2'-bipyridine

: 474363-03-6
N,N,N'-tris[(6-bromo-2,2'-bipyridine-5'-yl)methyl]-N'-p-nitrobenzylethylenediamine

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃; for 19h;
DOI:10.1055/s-2002-31968

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 474363-03-6
N,N,N'-tris[(6-bromo-2,2'-bipyridine-5'-yl)methyl]-N'-p-nitrobenzylethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / CH₂Cl₂ / 5 h / 0 - 20 °C

2: 74 percent / K₂CO₃ / acetonitrile / 19 h / 80 °C

With potassium carbonate; In dichloromethane; acetonitrile;
DOI:10.1055/s-2002-31968

Reference yield: 36.0%

: 64-17-5
ethanol

: 201230-82-2
carbon monoxide

: 474363-03-6
N,N,N'-tris[(6-bromo-2,2'-bipyridine-5'-yl)methyl]-N'-p-nitrobenzylethylenediamine

: N,N,N'-tris[(6-carboethoxy-2,2'-bipyridine-5'-yl)methyl]-N'-p-nitrobenzylethylenediamine dihydrochloride

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; at 80 ℃; for 96h; under 760 Torr;
DOI:10.1055/s-2002-31968