2-Propenoic acid, 2-methyl-, monoester with 2,2,4-trimethyl-1,3-pentanediol

Base Information

• Chemical Name: 2-Propenoic acid, 2-methyl-, monoester with 2,2,4-trimethyl-1,3-pentanediol
• CAS No.: 13283-45-9
• Molecular Formula: C₁₂H₂₂O₃
• Molecular Weight: 214.305
• Mol file: 13283-45-9.mol

Synonyms:Methacrylicacid, 3-hydroxy-2,2,4-trimethylpentyl ester (8CI);2,2,4-Trimethyl-1,3-pentanediol monomethacrylate

Chemical Property of 2-Propenoic acid, 2-methyl-, monoester with 2,2,4-trimethyl-1,3-pentanediol

Chemical Property:

Purity/Quality:

99.0%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Propenoic acid, 2-methyl-, monoester with 2,2,4-trimethyl-1,3-pentanediol

There total 2 articles about 2-Propenoic acid, 2-methyl-, monoester with 2,2,4-trimethyl-1,3-pentanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(methacryloyloxy)-2,2,4-trimethylpentyl 3-oxobutanoate (1381948-48-6) + 1-(methacryloyloxy)-2,2,4-trimethylpentan-3-yl 3-oxobutanoate (1381948-49-7) → 1-i-propyl-2,2-dimethyl-3-hydroxypropyl methacrylate + 2,2-dimethyl-3-hydroxy-4-methylpentyl methacrylate (13283-45-9) + acetone (67-64-1)

Guidance literature:

With water; at 90 ℃; for 96h; Reactivity;

Reference yield:

2,2,4-trimethylpentan-1,3-diol (144-19-4) + methacryloyl anhydride (760-93-0) → 1-i-propyl-2,2-dimethyl-3-hydroxypropyl methacrylate + 2,2-dimethyl-3-hydroxy-4-methylpentyl methacrylate (13283-45-9)

Guidance literature:

2,2,4-trimethylpentan-1,3-diol; methacryloyl anhydride; With dmap; In tetrahydrofuran; for 3h; Reflux;

With N-nitrosodiphenylamine; In tetrahydrofuran; at 85 - 90 ℃; under 0.5 Torr;

upstream raw materials:

2,2,4-trimethylpentan-1,3-diol

methacryloyl anhydride

3-(methacryloyloxy)-2,2,4-trimethylpentyl 3-oxobutanoate

1-(methacryloyloxy)-2,2,4-trimethylpentan-3-yl 3-oxobutanoate

Refernces