2-(3',4'-methylenedioxy-6'-ethyl)phenyl-3-(2''-oxoethyl)cyclopentanol benzoate

Base Information

Chemical Name:2-(3',4'-methylenedioxy-6'-ethyl)phenyl-3-(2''-oxoethyl)cyclopentanol benzoate
CAS No.:73116-30-0
Molecular Formula:C₂₃H₂₄O₅
Molecular Weight:380.441
Hs Code.:

Synonyms:2-(3',4'-methylenedioxy-6'-ethyl)phenyl-3-(2''-oxoethyl)cyclopentanol benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3',4'-methylenedioxy-6'-ethyl)phenyl-3-(2''-oxoethyl)cyclopentanol benzoate

Chemical Property:

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Technology Process of 2-(3',4'-methylenedioxy-6'-ethyl)phenyl-3-(2''-oxoethyl)cyclopentanol benzoate

There total 8 articles about 2-(3',4'-methylenedioxy-6'-ethyl)phenyl-3-(2''-oxoethyl)cyclopentanol benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 73135-73-6
2-(3',4'-methylenedioxy-6'-ethyl)phenyl-3-(2''-propenyl)cyclopentanol benzoate

: 73116-30-0
2-(3',4'-methylenedioxy-6'-ethyl)phenyl-3-(2''-oxoethyl)cyclopentanol benzoate

Guidance literature:: With sodium periodate; osmium(VIII) oxide;
DOI:10.1021/ja00523a029

Reference yield:

: 24316-19-6
cephalotaxine

: 73116-30-0
2-(3',4'-methylenedioxy-6'-ethyl)phenyl-3-(2''-oxoethyl)cyclopentanol benzoate

Guidance literature:: Multi-step reaction with 7 steps

1: 2.) 3percent sodium amalgam / 1.) methanol, ambient temperature, 24 h, 2.) ethanol, water, steam bath, 2 h

2: 2.) Rexyn 201 (OH^-), 3.) benzene

3: 99 percent / H₂ / platinum oxide / ethanol / Ambient temperature

4: 80 percent / NaBH₄ / ethanol / Ambient temperature

5: 1.) 30percent hydrogen peroxide / 1.) heated on a steam bath, 2.) 170 deg C, 0.06 - 0.03 mm

6: 91 percent / pyridine / 1.5 h / Ambient temperature

7: 66 percent / OsO₄-NaIO₄

With sodium tetrahydroborate; sodium periodate; sodium amalgam; osmium(VIII) oxide; Rexyn 201 (OH^-); hydrogen; dihydrogen peroxide; benzene; platinum(IV) oxide; In pyridine; ethanol;
DOI:10.1021/ja00523a029

Reference yield:

: 73116-27-5
2-(3',4'-methylenedioxy-6'-vinyl)phenyl-3-(3''-N,N-dimethylaminopropyl)cyclopentanone

: 73116-30-0
2-(3',4'-methylenedioxy-6'-ethyl)phenyl-3-(2''-oxoethyl)cyclopentanol benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / H₂ / platinum oxide / ethanol / Ambient temperature

2: 80 percent / NaBH₄ / ethanol / Ambient temperature

3: 1.) 30percent hydrogen peroxide / 1.) heated on a steam bath, 2.) 170 deg C, 0.06 - 0.03 mm

4: 91 percent / pyridine / 1.5 h / Ambient temperature

5: 66 percent / OsO₄-NaIO₄

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; hydrogen; dihydrogen peroxide; platinum(IV) oxide; In pyridine; ethanol;
DOI:10.1021/ja00523a029