1,4,10-trimethyl-9-(2,3,5,6-tetramethylphenyl)thioxanthenium perchlorate

Base Information

Chemical Name:1,4,10-trimethyl-9-(2,3,5,6-tetramethylphenyl)thioxanthenium perchlorate
CAS No.:91127-69-4
Molecular Formula:C₂₆H₂₉S*ClO₄
Molecular Weight:473.033
Hs Code.:

Synonyms:1,4,10-trimethyl-9-(2,3,5,6-tetramethylphenyl)thioxanthenium perchlorate

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Chemical Property of 1,4,10-trimethyl-9-(2,3,5,6-tetramethylphenyl)thioxanthenium perchlorate

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Technology Process of 1,4,10-trimethyl-9-(2,3,5,6-tetramethylphenyl)thioxanthenium perchlorate

There total 3 articles about 1,4,10-trimethyl-9-(2,3,5,6-tetramethylphenyl)thioxanthenium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 91127-81-0
1,4-dimethyl-9-(2,3,5,6-tetramethylphenyl)thioxanthene

: 74-88-4
methyl iodide

: 91127-69-4
1,4,10-trimethyl-9-(2,3,5,6-tetramethylphenyl)thioxanthenium perchlorate

Guidance literature:: With silver perchlorate; In 1,2-dichloro-ethane;
DOI:10.1021/jo00191a020

Reference yield:

: 1646-53-3
bromodurene

: 91127-69-4
1,4,10-trimethyl-9-(2,3,5,6-tetramethylphenyl)thioxanthenium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / Mg, I₂ / tetrahydrofuran; diethyl ether / 0.5 h / Heating

2: 71 percent / AgClO₄ / 1,2-dichloro-ethane

With iodine; silver perchlorate; magnesium; In tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1021/jo00191a020

Reference yield:

: 91127-87-6
1,4-dimethylthioxanthylium perchlorate

: 91127-69-4
1,4,10-trimethyl-9-(2,3,5,6-tetramethylphenyl)thioxanthenium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / Mg, I₂ / tetrahydrofuran; diethyl ether / 0.5 h / Heating

2: 71 percent / AgClO₄ / 1,2-dichloro-ethane

With iodine; silver perchlorate; magnesium; In tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1021/jo00191a020