ethyl 3-phenylhexanoate

Base Information

Chemical Name:ethyl 3-phenylhexanoate
CAS No.:72277-16-8
Molecular Formula:C₁₄H₂₀O₂
Molecular Weight:220.312
Hs Code.:

Synonyms:ethyl 3-phenylhexanoate

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Chemical Property of ethyl 3-phenylhexanoate

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Technology Process of ethyl 3-phenylhexanoate

There total 7 articles about ethyl 3-phenylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 54653-25-7
ethyl hex-5-enoate

: 143-66-8
sodium tetraphenyl borate

: 72277-16-8
ethyl 3-phenylhexanoate

Guidance literature:: acetylacetonato(1,5-cyclooctadiene)rhodium(I); biphephos; In water; toluene; at 100 ℃; for 20h; Product distribution / selectivity; Inert atmosphere; Sealed vessel;

Reference yield:

: 27829-72-7
ethyl (E)-hex-2-enoate

: 591-51-5
phenyllithium

: 72277-16-8
ethyl 3-phenylhexanoate

: ethyl 3-phenylhexanoate

Guidance literature:: phenyllithium; With Trimethyl borate; In diethyl ether; hexane; at -78 - -20 ℃; for 1.5h;

ethyl (E)-hex-2-enoate; With bis(ethylene)rhodium acetylacetonate; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); In 1,4-dioxane; diethyl ether; water; at 100 ℃; for 3h; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(99)00417-6

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 72277-16-8
ethyl 3-phenylhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / benzene / 6 h / Ambient temperature

2: 1.) LDA / 1.) THF, hexane, -78 deg C, 30 min

3: TsOH / 2 h / 78 °C

With toluene-4-sulfonic acid; lithium diisopropyl amide; In benzene;
DOI:10.1246/bcsj.55.224