2-(2-amino-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-(2-chloropyridin-3-yl)acetamide

Base Information

Chemical Name:2-(2-amino-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-(2-chloropyridin-3-yl)acetamide
CAS No.:1260403-04-0
Molecular Formula:C₁₆H₁₁Br₂ClN₄OS₂
Molecular Weight:534.683
Hs Code.:

Synonyms:2-(2-amino-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-(2-chloropyridin-3-yl)acetamide

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Chemical Property of 2-(2-amino-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-(2-chloropyridin-3-yl)acetamide

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Technology Process of 2-(2-amino-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-(2-chloropyridin-3-yl)acetamide

There total 4 articles about 2-(2-amino-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-(2-chloropyridin-3-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6298-19-7
2-chloro-3-aminopyridine

: C₁₁H₇Br₂ClN₂OS₂*ClH

: 1260403-04-0
2-(2-amino-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-(2-chloropyridin-3-yl)acetamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 10h; Cooling with ice;
DOI:10.1007/s12272-012-0604-y

Reference yield:

: 1385770-66-0
C₁₂H₁₁Br₃O₃S

: 1260403-04-0
2-(2-amino-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-(2-chloropyridin-3-yl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 20 °C

2: sodium hydroxide / dimethyl sulfoxide / 4 h / 20 °C

3: phosphorus pentachloride / diethyl ether / 5 h / 20 °C

4: triethylamine / dichloromethane / 10 h / 20 °C / Cooling with ice

With phosphorus pentachloride; triethylamine; sodium hydroxide; In diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1007/s12272-012-0604-y

Reference yield:

: 52167-36-9
2-chloro-1-(2,4-dibromophenyl)ethanone

: 1260403-04-0
2-(2-amino-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-(2-chloropyridin-3-yl)acetamide

Guidance literature:: Multi-step reaction with 6 steps

1: sodium carbonate / ethanol / 12 h / 20 °C

2: bromine / acetic acid / 8.5 h / 20 °C

3: ethanol / 20 °C

4: sodium hydroxide / dimethyl sulfoxide / 4 h / 20 °C

5: phosphorus pentachloride / diethyl ether / 5 h / 20 °C

6: triethylamine / dichloromethane / 10 h / 20 °C / Cooling with ice

With phosphorus pentachloride; bromine; sodium carbonate; triethylamine; sodium hydroxide; In diethyl ether; ethanol; dichloromethane; acetic acid; dimethyl sulfoxide;
DOI:10.1007/s12272-012-0604-y