methyl 3,6-anhydro-2-deoxy-4,5-O-isopropylidene-7-O-trityl-D-allo-heptanoate

Base Information

Chemical Name:methyl 3,6-anhydro-2-deoxy-4,5-O-isopropylidene-7-O-trityl-D-allo-heptanoate
CAS No.:56752-57-9
Molecular Formula:C₃₀H₃₂O₆
Molecular Weight:488.58
Hs Code.:

Synonyms:methyl 3,6-anhydro-2-deoxy-4,5-O-isopropylidene-7-O-trityl-D-allo-heptanoate

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Chemical Property of methyl 3,6-anhydro-2-deoxy-4,5-O-isopropylidene-7-O-trityl-D-allo-heptanoate

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Technology Process of methyl 3,6-anhydro-2-deoxy-4,5-O-isopropylidene-7-O-trityl-D-allo-heptanoate

There total 1 articles about methyl 3,6-anhydro-2-deoxy-4,5-O-isopropylidene-7-O-trityl-D-allo-heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56752-57-9
methyl 3,6-anhydro-2-deoxy-4,5-O-isopropylidene-7-O-trityl-D-allo-heptanoate

Guidance literature:: aus 7a, 8a in Acetonitril;
DOI:10.1021/ja00849a023

Reference yield: 83.0%

: 56752-57-9
methyl 3,6-anhydro-2-deoxy-4,5-O-isopropylidene-7-O-trityl-D-allo-heptanoate

: 73485-68-4
2-(2,3-O-isopropylidene-5-O-trityl-β-D-ribofuranosyl)ethanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at -20 - 20 ℃; for 1.33333h;
DOI:10.1246/bcsj.56.2700

Reference yield:

: 56752-57-9
methyl 3,6-anhydro-2-deoxy-4,5-O-isopropylidene-7-O-trityl-D-allo-heptanoate

: 73485-70-8
4,7-anhydro-2,3-dideoxy-5,6-O-isopropylidene-8-O-trityl-D-allo-octononitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / LiAlH₄ / tetrahydrofuran / 1.33 h / -20 - 20 °C

2: 63 percent / pyridine / 15 h / 0 °C

3: 67 percent / perhydrodibenzo-18-crown-6 / acetonitrile / 15 h / Heating

With pyridine; perhydrodibenzo-18-crown-6; lithium aluminium tetrahydride; In tetrahydrofuran; acetonitrile;
DOI:10.1246/bcsj.56.2700