1-<2-(3,4-Dimethoxyphenyl)-ethyl>-2,3-dioxo-2,3,3a,4,5,6-hexahydroindole

Base Information

Chemical Name:1-<2-(3,4-Dimethoxyphenyl)-ethyl>-2,3-dioxo-2,3,3a,4,5,6-hexahydroindole
CAS No.:78140-32-6
Molecular Formula:C₁₈H₂₁NO₄
Molecular Weight:315.369
Hs Code.:

Synonyms:1-<2-(3,4-Dimethoxyphenyl)-ethyl>-2,3-dioxo-2,3,3a,4,5,6-hexahydroindole

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Chemical Property of 1-<2-(3,4-Dimethoxyphenyl)-ethyl>-2,3-dioxo-2,3,3a,4,5,6-hexahydroindole

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Technology Process of 1-<2-(3,4-Dimethoxyphenyl)-ethyl>-2,3-dioxo-2,3,3a,4,5,6-hexahydroindole

There total 5 articles about 1-<2-(3,4-Dimethoxyphenyl)-ethyl>-2,3-dioxo-2,3,3a,4,5,6-hexahydroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 77638-68-7,78140-28-0
(S)-1-[2-(3,4-Dimethoxy-phenyl)-ethyl]-2,3-dioxo-1,2,3,4,5,6-hexahydro-indole-3a-carboxylic acid ethyl ester

: 78140-32-6
1-<2-(3,4-Dimethoxyphenyl)-ethyl>-2,3-dioxo-2,3,3a,4,5,6-hexahydroindole

Guidance literature:: With magnesium chloride; In dimethyl sulfoxide; at 150 ℃; for 1h;
DOI:10.1055/s-1981-29353

Reference yield: 54.0%

: 77638-68-7
1-[2-(3,4-Dimethoxy-phenyl)-ethyl]-2,3-dioxo-1,2,3,4,5,6-hexahydro-indole-3a-carboxylic acid ethyl ester

: 78140-32-6
1-<2-(3,4-Dimethoxyphenyl)-ethyl>-2,3-dioxo-2,3,3a,4,5,6-hexahydroindole

Guidance literature:: With magnesium chloride; In dimethyl sulfoxide; at 150 - 155 ℃; for 2h;
DOI:10.1248/cpb.38.1462

Reference yield:

: 77638-67-6
2-[2-(3,4-Dimethoxy-phenyl)-ethylamino]-cyclohex-1-enecarboxylic acid ethyl ester

: 78140-32-6
1-<2-(3,4-Dimethoxyphenyl)-ethyl>-2,3-dioxo-2,3,3a,4,5,6-hexahydroindole

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 0.5 h / 0 °C

2: 54 percent / MgCl₂ / dimethylsulfoxide / 2 h / 150 - 155 °C

With magnesium chloride; In dimethyl sulfoxide; benzene;
DOI:10.1248/cpb.38.1462