O-tert-butyltyrosylglycylglycine ethyl ester

Base Information

Chemical Name:O-tert-butyltyrosylglycylglycine ethyl ester
CAS No.:107941-82-2
Molecular Formula:C₁₉H₂₉N₃O₅
Molecular Weight:379.456
Hs Code.:

Synonyms:O-tert-butyltyrosylglycylglycine ethyl ester

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Chemical Property of O-tert-butyltyrosylglycylglycine ethyl ester

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Technology Process of O-tert-butyltyrosylglycylglycine ethyl ester

There total 4 articles about O-tert-butyltyrosylglycylglycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.5%

: 107941-81-1
N-(benzyloxycarbonyl)-O-tert-butyltyrosylglycylglycine ethyl ester

: 107941-82-2
O-tert-butyltyrosylglycylglycine ethyl ester

Guidance literature:: With hydrogen; ammonium formate; palladium on activated charcoal; In methanol; for 0.666667h;
DOI:10.1021/jm00390a005

Reference yield:

: 5545-54-0
N-(benzyloxycarbonyl)-O-(1,1-dimethylethyl)-L-tyrosine

: 107941-82-2
O-tert-butyltyrosylglycylglycine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) isobutyl chloroformate, N-methylmorpholine / 1.) THF, 2.) THF, DMF

2: 86.5 percent / ammonium formate, H₂ / 10percent Pd/C / methanol / 0.67 h

With 4-methyl-morpholine; hydrogen; ammonium formate; isobutyl chloroformate; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00390a005

Reference yield:

: 16679-94-0
N-[(phenylmethoxy)carbonyl]-L-tyrosine

: 107941-82-2
O-tert-butyltyrosylglycylglycine ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: conc. H₂SO₄ / CH₂Cl₂

2: 89.7 percent / 0.25 N NaOH / tetrahydrofuran / 25 °C

3: 1.) isobutyl chloroformate, N-methylmorpholine / 1.) THF, 2.) THF, DMF

4: 86.5 percent / ammonium formate, H₂ / 10percent Pd/C / methanol / 0.67 h

With 4-methyl-morpholine; sodium hydroxide; sulfuric acid; hydrogen; ammonium formate; isobutyl chloroformate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00390a005