4-{3-[4-(3-{4-[amino(propoxycarbonylimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-(propoxycarbonyl)benzamidine

Base Information

Chemical Name:4-{3-[4-(3-{4-[amino(propoxycarbonylimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-(propoxycarbonyl)benzamidine
CAS No.:943150-82-1
Molecular Formula:C₃₃H₄₇N₅O₆
Molecular Weight:609.766
Hs Code.:

Synonyms:4-{3-[4-(3-{4-[amino(propoxycarbonylimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-(propoxycarbonyl)benzamidine

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Chemical Property of 4-{3-[4-(3-{4-[amino(propoxycarbonylimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-(propoxycarbonyl)benzamidine

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Technology Process of 4-{3-[4-(3-{4-[amino(propoxycarbonylimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-(propoxycarbonyl)benzamidine

There total 9 articles about 4-{3-[4-(3-{4-[amino(propoxycarbonylimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-(propoxycarbonyl)benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 873546-31-7
4-{3-[1-(3-{4-[amino(imino)methyl]phenoxy}propyl)piperidin-4-yl]propoxy}benzamidine

: 67036-12-8
n-propyl 4-nitrophenyl carbonate

: 943150-82-1
4-{3-[4-(3-{4-[amino(propoxycarbonylimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-(propoxycarbonyl)benzamidine

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield:

: 873546-31-7
4-{3-[1-(3-{4-[amino(imino)methyl]phenoxy}propyl)piperidin-4-yl]propoxy}benzamidine

aqueous sodium chloride: aqueous sodium chloride

: 4-nitrophenylpropyl carbonate

: 943150-82-1
4-{3-[4-(3-{4-[amino(propoxycarbonylimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-(propoxycarbonyl)benzamidine

Guidance literature:: With potassium carbonate; In chloroform; water; N,N-dimethyl-formamide;

Reference yield:

: 873546-30-6
4-{3-[4-(3-{4-[amino(hydroxyimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-hydroxybenzamidine

: 943150-82-1
4-{3-[4-(3-{4-[amino(propoxycarbonylimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-(propoxycarbonyl)benzamidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 0.67 h / 20 °C

2.1: hydrogen / 5%-palladium/activated carbon / acetic acid / 2.25 h

2.3: pH 12.5

3.1: N,N-dimethyl-formamide / 4 h / 20 °C

With hydrogen; 5%-palladium/activated carbon; In acetic acid; N,N-dimethyl-formamide;