Acetic acid, 1,1'-[1,4-piperidinediylbis(3,1-propanediyloxy-4,1-phenylenecarbonimidoylazanylidene)] ester

Base Information

Chemical Name:Acetic acid, 1,1'-[1,4-piperidinediylbis(3,1-propanediyloxy-4,1-phenylenecarbonimidoylazanylidene)] ester
CAS No.:873546-74-8
Molecular Formula:C29H39N5O6
Molecular Weight:553.65
Hs Code.:

Synonyms:Benzenecarboximidamide, 4,4'-[1,4-piperidinediylbis(3,1-propanediyloxy)]bis[N-(acetyloxy)- (9CI);

Suppliers and Price of Acetic acid, 1,1'-[1,4-piperidinediylbis(3,1-propanediyloxy-4,1-phenylenecarbonimidoylazanylidene)] ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid, 1,1'-[1,4-piperidinediylbis(3,1-propanediyloxy-4,1-phenylenecarbonimidoylazanylidene)] ester

Chemical Property:

PSA：151.06000
LogP:4.73200

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Acetic acid, 1,1'-[1,4-piperidinediylbis(3,1-propanediyloxy-4,1-phenylenecarbonimidoylazanylidene)] ester

There total 7 articles about Acetic acid, 1,1'-[1,4-piperidinediylbis(3,1-propanediyloxy-4,1-phenylenecarbonimidoylazanylidene)] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 873546-30-6
4-{3-[4-(3-{4-[amino(hydroxyimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-hydroxybenzamidine

: 108-24-7
acetic anhydride

: 873546-74-8
4-{3-[4-(3-{4-[amino(acetyloxyimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}benzamide O-acetyloxime

Guidance literature:: In acetic acid; at 20 ℃; for 0.666667h;

Reference yield:

: 873546-30-6
4-{3-[4-(3-{4-[amino(hydroxyimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}-N'-hydroxybenzamidine

: 108-24-7
acetic anhydride

: 64-19-7,77671-22-8
acetic acid

: 873546-74-8
4-{3-[4-(3-{4-[amino(acetyloxyimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}benzamide O-acetyloxime

Guidance literature:: at 20 ℃; for 0.666667 - 1.33333h; Product distribution / selectivity;

Reference yield:

: 873546-88-4
4-{3-[4-(3-hydroxypropyl)-1-piperidinyl]propoxy}benzonitrile

: 873546-74-8
4-{3-[4-(3-{4-[amino(acetyloxyimino)methyl]phenoxy}propyl)-1-piperidinyl]propoxy}benzamide O-acetyloxime

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / 1.17 h / 20 °C

2: potassium carbonate / dimethyl sulfoxide / 2 h / 20 - 60 °C

3: hydroxylamine / water; dimethyl sulfoxide / 19 h / 50 °C

4: acetic acid / 0.67 h / 20 °C

With hydroxylamine; potassium carbonate; triethylamine; In tetrahydrofuran; water; acetic acid; dimethyl sulfoxide;