C₃₃H₃₉FN₆O₅S

Base Information

Chemical Name:C₃₃H₃₉FN₆O₅S
CAS No.:868286-95-7
Molecular Formula:C₃₃H₃₉FN₆O₅S
Molecular Weight:650.774
Hs Code.:

C<sub>33</sub>H<sub>39</sub>FN<sub>6</sub>O<sub>5</sub>S

Synonyms:C₃₃H₃₉FN₆O₅S

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Chemical Property of C₃₃H₃₉FN₆O₅S

Chemical Property:

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Technology Process of C₃₃H₃₉FN₆O₅S

There total 15 articles about C₃₃H₃₉FN₆O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 868286-25-3
(R)-tert-butyl (1-hydrazinyl-2-methyl-1-oxo-3-phenylpropan-2-yl)carbamate

: 1048666-17-6
ethyl-3-({[(1R)-1-(4-fluorophenyl)ethyl]amino}carbonyl)-5-[methyl(methylsulfonyl)amino]benzenecarboximidoate

: 868286-95-7
C₃₃H₃₉FN₆O₅S

Guidance literature:: In ethanol; at 0 ℃; for 43h; Heating / reflux;

Reference yield:

: 695216-00-3
3-[(methylsulfonyl)amino]-5-nitrobenzoic acid methyl ester

: 868286-95-7
C₃₃H₃₉FN₆O₅S

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 3 h / 20 °C

2.1: methanol; sodium hydroxide / tetrahydrofuran / 1.5 h / 20 °C

2.2: 20 °C / pH < 1

3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 65 h / 20 °C

4.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h

5.1: tetrafluoroboric acid / water; acetonitrile / 0.67 h / 0 - 20 °C

5.2: 1 h / 0 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / DMF (N,N-dimethyl-formamide) / 0.5 h / 180 °C / Microwave

7.1: hydroxylamine hydrochloride; water; potassium carbonate; isopropyl alcohol / 0.08 h / 130 °C / Microwave

8.1: hydrogenchloride / dichloromethane / 20.53 h / 0 - 20 °C

8.2: 0.02 h / 0 °C

9.1: ethanol / 43 h / 0 °C / Heating / reflux

With hydrogenchloride; methanol; sodium hydroxide; tetrafluoroboric acid; 1-hydroxy-7-aza-benzotriazole; hydroxylamine hydrochloride; water; hydrogen; sodium hydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isopropyl alcohol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 695216-01-4
3-[methyl(methylsulfonyl)amino]-5-nitrobenzoic acid methyl ester

: 868286-95-7
C₃₃H₃₉FN₆O₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: methanol; sodium hydroxide / tetrahydrofuran / 1.5 h / 20 °C

1.2: 20 °C / pH < 1

2.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 65 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h

4.1: tetrafluoroboric acid / water; acetonitrile / 0.67 h / 0 - 20 °C

4.2: 1 h / 0 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / DMF (N,N-dimethyl-formamide) / 0.5 h / 180 °C / Microwave

6.1: hydroxylamine hydrochloride; water; potassium carbonate; isopropyl alcohol / 0.08 h / 130 °C / Microwave

7.1: hydrogenchloride / dichloromethane / 20.53 h / 0 - 20 °C

7.2: 0.02 h / 0 °C

8.1: ethanol / 43 h / 0 °C / Heating / reflux

With hydrogenchloride; methanol; sodium hydroxide; tetrafluoroboric acid; 1-hydroxy-7-aza-benzotriazole; hydroxylamine hydrochloride; water; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isopropyl alcohol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; acetonitrile;