(3'S,5'R,6'R)-N⁴-benzoyl-1-{2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl}cytosine

Base Information

• Chemical Name: (3'S,5'R,6'R)-N⁴-benzoyl-1-{2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl}cytosine
• CAS No.: 918886-48-3
• Molecular Formula: C₄₀H₃₇N₃O₇
• Molecular Weight: 671.75

Synonyms:(3'S,5'R,6'R)-N⁴-benzoyl-1-{2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl}cytosine

Chemical Property of (3'S,5'R,6'R)-N⁴-benzoyl-1-{2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl}cytosine

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Technology Process of (3'S,5'R,6'R)-N⁴-benzoyl-1-{2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl}cytosine

There total 1 articles about (3'S,5'R,6'R)-N⁴-benzoyl-1-{2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl}cytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(3'S,5'R,6'S)-N4-benzoyl-1-(2'-deoxy-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl)cytosine (918886-44-9) + 4,4’-dimethoxytrityl trifluoromethanesulfonate (239808-67-4) → (3'S,5'R,6'R)-N4-benzoyl-1-{2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl}cytosine (918886-48-3)

Guidance literature:

In pyridine; at 20 ℃; for 4h;

DOI:10.1002/chem.200600597

Reference yield: 71.0%

(3'S,5'R,6'R)-N4-benzoyl-1-{2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl}cytosine (918886-48-3) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → (5'R,6'S)-N4-benzoyl-1-{3'-O-[(2-cyanoethoxy)(diisopropylamino)phosphino]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl}cytosine

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 2h;

DOI:10.1002/chem.200600597

upstream raw materials:

(3'S,5'R,6'S)-N⁴-benzoyl-1-(2'-deoxy-3',5'-ethano-5',6'-methano-α-D-ribofuranosyl)cytosine

4,4’-dimethoxytrityl trifluoromethanesulfonate

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