N-(Boc)-2',3'-dimercapto-4',5'-dimethoxyphenethylamine

Base Information

Chemical Name:N-(Boc)-2',3'-dimercapto-4',5'-dimethoxyphenethylamine
CAS No.:478809-62-0
Molecular Formula:C₁₅H₂₃NO₄S₂
Molecular Weight:345.484
Hs Code.:

Synonyms:N-(Boc)-2',3'-dimercapto-4',5'-dimethoxyphenethylamine

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Chemical Property of N-(Boc)-2',3'-dimercapto-4',5'-dimethoxyphenethylamine

Chemical Property:

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Technology Process of N-(Boc)-2',3'-dimercapto-4',5'-dimethoxyphenethylamine

There total 7 articles about N-(Boc)-2',3'-dimercapto-4',5'-dimethoxyphenethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 478809-61-9
N-(Boc)-2',3'-bis(n-butylsulfanyl)-4',5'-dimethoxyphenethylamine

: 478809-62-0
N-(Boc)-2',3'-dimercapto-4',5'-dimethoxyphenethylamine

Guidance literature:: With ammonia; lithium; In tetrahydrofuran; for 1h;
DOI:10.1021/ja020531i

Reference yield:

: 2973-75-3
5,6-dibromo-4-hydroxy-3-methoxybenzaldehyde

: 478809-62-0
N-(Boc)-2',3'-dimercapto-4',5'-dimethoxyphenethylamine

Guidance literature:: Multi-step reaction with 6 steps

1.1: 65 percent / quinoline; pyridine / 2 h / 160 °C

2.1: 99 percent / K₂CO₃; tetra-n-butylammonium iodide / tetrahydrofuran; H₂O / Heating

3.1: 78 percent / NH₄OAc / acetic acid / 8 h / 20 °C / ultrasonic bath

4.1: LiAlH₄ / diethyl ether / 1.5 h / Heating

4.2: aq. HCl / diethyl ether

5.1: 52 percent / TEA / tetrahydrofuran / 2 h / Heating

6.1: 100 percent / Li; NH₃ / tetrahydrofuran / 1 h

With pyridine; quinoline; lithium aluminium tetrahydride; TEA; ammonium acetate; ammonia; tetra-(n-butyl)ammonium iodide; lithium; potassium carbonate; In tetrahydrofuran; diethyl ether; water; acetic acid;
DOI:10.1021/ja020531i

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 478809-62-0
N-(Boc)-2',3'-dimercapto-4',5'-dimethoxyphenethylamine

Guidance literature:: Multi-step reaction with 7 steps

1.1: 78 percent / bromine; iron / acetic acid / Heating

2.1: 65 percent / quinoline; pyridine / 2 h / 160 °C

3.1: 99 percent / K₂CO₃; tetra-n-butylammonium iodide / tetrahydrofuran; H₂O / Heating

4.1: 78 percent / NH₄OAc / acetic acid / 8 h / 20 °C / ultrasonic bath

5.1: LiAlH₄ / diethyl ether / 1.5 h / Heating

5.2: aq. HCl / diethyl ether

6.1: 52 percent / TEA / tetrahydrofuran / 2 h / Heating

7.1: 100 percent / Li; NH₃ / tetrahydrofuran / 1 h

With pyridine; quinoline; lithium aluminium tetrahydride; TEA; ammonium acetate; ammonia; bromine; tetra-(n-butyl)ammonium iodide; lithium; iron; potassium carbonate; In tetrahydrofuran; diethyl ether; water; acetic acid;
DOI:10.1021/ja020531i