Technology Process of N-(Boc)-2',3'-bis(n-butylsulfanyl)-4',5'-dimethoxyphenethylamine
There total 6 articles about N-(Boc)-2',3'-bis(n-butylsulfanyl)-4',5'-dimethoxyphenethylamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
TEA;
In
tetrahydrofuran;
for 2h;
Heating;
DOI:10.1021/ja020531i
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 65 percent / quinoline; pyridine / 2 h / 160 °C
2.1: 99 percent / K2CO3; tetra-n-butylammonium iodide / tetrahydrofuran; H2O / Heating
3.1: 78 percent / NH4OAc / acetic acid / 8 h / 20 °C / ultrasonic bath
4.1: LiAlH4 / diethyl ether / 1.5 h / Heating
4.2: aq. HCl / diethyl ether
5.1: 52 percent / TEA / tetrahydrofuran / 2 h / Heating
With
pyridine; quinoline; lithium aluminium tetrahydride; TEA; ammonium acetate; tetra-(n-butyl)ammonium iodide; potassium carbonate;
In
tetrahydrofuran; diethyl ether; water; acetic acid;
DOI:10.1021/ja020531i
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 78 percent / bromine; iron / acetic acid / Heating
2.1: 65 percent / quinoline; pyridine / 2 h / 160 °C
3.1: 99 percent / K2CO3; tetra-n-butylammonium iodide / tetrahydrofuran; H2O / Heating
4.1: 78 percent / NH4OAc / acetic acid / 8 h / 20 °C / ultrasonic bath
5.1: LiAlH4 / diethyl ether / 1.5 h / Heating
5.2: aq. HCl / diethyl ether
6.1: 52 percent / TEA / tetrahydrofuran / 2 h / Heating
With
pyridine; quinoline; lithium aluminium tetrahydride; TEA; ammonium acetate; bromine; tetra-(n-butyl)ammonium iodide; iron; potassium carbonate;
In
tetrahydrofuran; diethyl ether; water; acetic acid;
DOI:10.1021/ja020531i
