1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-D-erythro-pent-1-enitol

Base Information

Chemical Name:1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-D-erythro-pent-1-enitol
CAS No.:127761-83-5
Molecular Formula:C₂₁H₂₆O₃Si
Molecular Weight:354.521
Hs Code.:

Synonyms:1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-D-erythro-pent-1-enitol

Suppliers and Price of 1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-D-erythro-pent-1-enitol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-D-erythro-pent-1-enitol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-D-erythro-pent-1-enitol

There total 5 articles about 1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-D-erythro-pent-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 101527-40-6
5'-O-tert-butyldiphenylsilylthymidine

: 127761-83-5
1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-D-erythro-pent-1-enitol

Guidance literature:: With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane; for 4h; Heating;
DOI:10.1021/jo970947s

Reference yield: 74.0%

: 127791-68-8
1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-3-O-(trimethylsilyl)-D-erythro-pent-1-enitol

: 127761-83-5
1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-D-erythro-pent-1-enitol

Guidance literature:: With ammonia; In methanol; at 20 ℃; for 48h;
DOI:10.1007/s00706-005-0342-7

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 127761-83-5
1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-D-erythro-pent-1-enitol

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 24 h

2: 91 percent / HMDS, (NH₄)2SO₄ / 4 h / Heating

With 1H-imidazole; ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane; In N,N-dimethyl-formamide;
DOI:10.1021/jo970947s