2-((1-(4-(4-(2-(methacryloyloxy)ethylcarbamoyloxy)butoxy)-5-methoxy-2-nitro-phenyl)ethoxy)carbonylamino)ethyl methacrylate

Base Information

Chemical Name:2-((1-(4-(4-(2-(methacryloyloxy)ethylcarbamoyloxy)butoxy)-5-methoxy-2-nitro-phenyl)ethoxy)carbonylamino)ethyl methacrylate
CAS No.:1269794-14-0
Molecular Formula:C₂₇H₃₇N₃O₁₂
Molecular Weight:595.604
Hs Code.:

Synonyms:2-((1-(4-(4-(2-(methacryloyloxy)ethylcarbamoyloxy)butoxy)-5-methoxy-2-nitro-phenyl)ethoxy)carbonylamino)ethyl methacrylate

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Chemical Property of 2-((1-(4-(4-(2-(methacryloyloxy)ethylcarbamoyloxy)butoxy)-5-methoxy-2-nitro-phenyl)ethoxy)carbonylamino)ethyl methacrylate

Chemical Property:

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Technology Process of 2-((1-(4-(4-(2-(methacryloyloxy)ethylcarbamoyloxy)butoxy)-5-methoxy-2-nitro-phenyl)ethoxy)carbonylamino)ethyl methacrylate

There total 7 articles about 2-((1-(4-(4-(2-(methacryloyloxy)ethylcarbamoyloxy)butoxy)-5-methoxy-2-nitro-phenyl)ethoxy)carbonylamino)ethyl methacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 30674-80-7
2-Isocyanatoethyl methacrylate

: 1334290-05-9
4-(4-(1-hydroxyethyl)-2-methoxy-5-nitrophenoxy)butan-1-ol

: 1269794-14-0
2-((1-(4-(4-(2-(methacryloyloxy)ethylcarbamoyloxy)butoxy)-5-methoxy-2-nitro-phenyl)ethoxy)carbonylamino)ethyl methacrylate

Guidance literature:: With dibutyltin dilaurate; In tetrahydrofuran; at 65 ℃; for 48h;
DOI:10.1021/ma201706r

Reference yield:

: 30674-80-7
2-Isocyanatoethyl methacrylate

: 175281-76-2
4-[4-(1-hydroxyethyl)-2-methoxy-5-nitrophenoxy]butanoic acid

: 1269794-14-0
2-((1-(4-(4-(2-(methacryloyloxy)ethylcarbamoyloxy)butoxy)-5-methoxy-2-nitro-phenyl)ethoxy)carbonylamino)ethyl methacrylate

Guidance literature:: With dibutyltin dilaurate; In tetrahydrofuran; at 65 ℃; for 48h; Inert atmosphere;

Reference yield:

: 182297-45-6
methyl 4-(4-acetyl-2-methoxy-5-nitrophenoxy)butyrate

: 1269794-14-0
2-((1-(4-(4-(2-(methacryloyloxy)ethylcarbamoyloxy)butoxy)-5-methoxy-2-nitro-phenyl)ethoxy)carbonylamino)ethyl methacrylate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / tetrahydrofuran; methanol / 16 h / 25 °C

2: sodium hydroxide / tetrahydrofuran; methanol / 7 h / 25 °C

3: borane-THF / tetrahydrofuran / 19 h / 0 - 40 °C

4: dibutyltin dilaurate / tetrahydrofuran / 48 h / 65 °C

With sodium tetrahydroborate; borane-THF; dibutyltin dilaurate; sodium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1021/ma201706r