Technology Process of C19H30FNO6S
There total 7 articles about C19H30FNO6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: silver nitrate / diethyl ether / 22 h / 0 - 20 °C
2.1: aluminum (III) chloride / 1,2-dichloro-ethane / 12.33 h / 0 - 20 °C
2.2: Cooling with ice
3.1: trifluoroacetic acid; triethylsilane / 5 h / 20 °C
4.1: sodium hydroxide / 1,4-dioxane; ethanol; water / 16 h / 20 °C
5.1: thionyl chloride / dichloromethane / 5 h / 20 °C
6.1: sodium periodate / ruthenium trichloride / dichloromethane; acetonitrile; water / 2 h / 20 °C
7.1: tetramethylammonium fluoride / acetonitrile / 0.17 h / Reflux
With
triethylsilane; aluminum (III) chloride; sodium periodate; thionyl chloride; tetramethylammonium fluoride; silver nitrate; trifluoroacetic acid; sodium hydroxide;
ruthenium trichloride;
In
1,4-dioxane; diethyl ether; ethanol; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;
- Guidance literature:
-
With
tetramethylammonium fluoride;
In
acetonitrile;
for 0.166667h;
Product distribution / selectivity;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / dichloromethane / 5 h / 20 °C
2: sodium periodate / ruthenium trichloride / dichloromethane; acetonitrile; water / 2 h / 20 °C
3: tetramethylammonium fluoride / acetonitrile / 0.17 h / Reflux
With
sodium periodate; thionyl chloride; tetramethylammonium fluoride;
ruthenium trichloride;
In
dichloromethane; water; acetonitrile;
