benzyl tert-butyl {[5-(hydroxymethyl)-1,3-phenylene]dipropane-3,1-diyl}bis[carbamate]

Base Information

Chemical Name:benzyl tert-butyl {[5-(hydroxymethyl)-1,3-phenylene]dipropane-3,1-diyl}bis[carbamate]
CAS No.:807341-84-0
Molecular Formula:C₂₆H₃₆N₂O₅
Molecular Weight:456.582
Hs Code.:

Synonyms:benzyl tert-butyl {[5-(hydroxymethyl)-1,3-phenylene]dipropane-3,1-diyl}bis[carbamate]

Suppliers and Price of benzyl tert-butyl {[5-(hydroxymethyl)-1,3-phenylene]dipropane-3,1-diyl}bis[carbamate]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl tert-butyl {[5-(hydroxymethyl)-1,3-phenylene]dipropane-3,1-diyl}bis[carbamate]

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl tert-butyl {[5-(hydroxymethyl)-1,3-phenylene]dipropane-3,1-diyl}bis[carbamate]

There total 4 articles about benzyl tert-butyl {[5-(hydroxymethyl)-1,3-phenylene]dipropane-3,1-diyl}bis[carbamate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 349559-91-7
ethyl 3-{3-{[(benzyloxy)carbonyl]amino}propyl}-5-{3-{[(tert-butoxy)carbonyl]amino}propyl}benzoate

: 807341-84-0
benzyl tert-butyl {[5-(hydroxymethyl)-1,3-phenylene]dipropane-3,1-diyl}bis[carbamate]

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 8.5h; cooling;
DOI:10.1002/hlca.200690246

Reference yield:

: 870177-64-3
ethyl 3-bromo-5-{3-{[(benzyloxy)carbonyl]amino}propyl}benzoate

: 807341-84-0
benzyl tert-butyl {[5-(hydroxymethyl)-1,3-phenylene]dipropane-3,1-diyl}bis[carbamate]

Guidance literature:: Multi-step reaction with 2 steps

1.1: 9-BBN / toluene / 12 h / 20 °C

1.2: 86 percent / aq. KOH / Pd(PPh₃)4 / toluene / 14 h / 100 °C

2.1: 81 percent / LiAlH₄ / tetrahydrofuran / 8.5 h / cooling

With lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; toluene; 1.2: Suzuki-Miyaura cross-coupling;
DOI:10.1002/hlca.200690246

Reference yield:

: 5041-33-8
N-(Benzyloxycarbonyl)allylamine

: 807341-84-0
benzyl tert-butyl {[5-(hydroxymethyl)-1,3-phenylene]dipropane-3,1-diyl}bis[carbamate]

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9-BBN / toluene / 12 h / 20 °C

1.2: 66 percent / aq. KOH / Pd(PPh₃)4 / toluene / 48 h / 60 °C

2.1: 9-BBN / toluene / 12 h / 20 °C

2.2: 86 percent / aq. KOH / Pd(PPh₃)4 / toluene / 14 h / 100 °C

3.1: 81 percent / LiAlH₄ / tetrahydrofuran / 8.5 h / cooling

With lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; toluene; 1.2: Suzuki-Miyaura cross-coupling / 2.2: Suzuki-Miyaura cross-coupling;
DOI:10.1002/hlca.200690246