diethyl hept-6-en-1-ylphosphonate

Base Information

Chemical Name:diethyl hept-6-en-1-ylphosphonate
CAS No.:141917-82-0
Molecular Formula:C₁₁H₂₃O₃P
Molecular Weight:234.276
Hs Code.:

Synonyms:diethyl hept-6-en-1-ylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl hept-6-en-1-ylphosphonate

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Technology Process of diethyl hept-6-en-1-ylphosphonate

There total 1 articles about diethyl hept-6-en-1-ylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 4117-09-3
7-bromo-hept-1-ene

: 122-52-1
triethyl phosphite

: 141917-82-0
diethyl hept-6-en-1-ylphosphonate

Guidance literature:: for 16h; Heating;
DOI:10.1021/jm950736k

Reference yield: 67.0%

: (4-chlorophenyl)(5,5-dimethyl-2-oxido-1,3,2-dioxaphosphinan-2-yl)methanone

: 141917-82-0
diethyl hept-6-en-1-ylphosphonate

: diethyl (7-(4-chlorophenyl)-6-methyl-7-oxoheptyl)phosphonate

Guidance literature:: With tert.-butylhydroperoxide; [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II); phenylsilane; Selectfluor; In decane; isopropyl alcohol; at 22 ℃; for 12h; regioselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1021/jacs.1c02629

Reference yield: 61.0%

: (2,2’-bipyridine)Zn(CF₃)₂

: 133745-75-2
N-fluorobis(benzenesulfon)imide

: 141917-82-0
diethyl hept-6-en-1-ylphosphonate

: diethyl (7,7,7-trifluoro-6-((N-(phenylsulfonyl)phenylsulfonamido)methyl)-heptyl)phosphonate

Guidance literature:: With zinc trifluoromethanesulfonate; copper(II) bis(trifluoromethanesulfonate); lithium dimethylacetate; at 0 - 20 ℃; for 24h; regioselective reaction; Inert atmosphere; Glovebox;
DOI:10.1021/jacs.9b06141