2,6-Dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3H)-yl)benzeneacetaMide

Base Information

• Chemical Name: 2,6-Dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3H)-yl)benzeneacetaMide
• CAS No.: 112206-56-1
• Molecular Formula: C₁₇H₁₁Cl₃N₄O₃
• Molecular Weight: 425.658
• Mol file: 112206-56-1.mol

Synonyms:2,6-dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3 H)-yl)benzeneacetamide

Chemical Property of 2,6-Dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3H)-yl)benzeneacetaMide

Chemical Property:

• Melting Point: >278°C (dec.)
• Storage Temp.: Refrigerator
• Solubility.: DMSO

Purity/Quality:

2,6-Dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3H)-yl)benzeneacetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 2,6-Dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3H)-yl)benzeneacetamide is an anticoccidial trazine intermediate in the synthesis of Diclazuril (D436200), an antiprotozoal agent that acts upon Coccidia parasites.

Technology Process of 2,6-Dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3H)-yl)benzeneacetaMide

There total 1 articles about 2,6-Dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3H)-yl)benzeneacetaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3H)-yl)benzeneacetonitrile (101831-36-1) + chloroform (67-66-3,8013-54-5) → 2-chloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3 H)-yl)-benzeneacetamide + 2,6-dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3 H)-yl)benzeneacetamide (112206-56-1)

Guidance literature:

With sulfuric acid; In methanol; di-isopropyl ether; water;

Reference yield: 28.0%

2,6-dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3 H)-yl)benzeneacetamide (112206-56-1) → 2-[3,5-dichloro-4-(4-chlorobenzyl)phenyl]-1,2,4-triazine-3,5(2H,4H)-dione (133648-80-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 100 ℃; for 4h;

DOI:10.1021/jm00110a023

Reference yield:

2,6-dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3 H)-yl)benzeneacetamide (112206-56-1) + toluene (108-88-3,15644-74-3,16713-13-6) → 2,6-dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3 H)-yl)benzeneacetic acid (112206-58-3)

Guidance literature:

With hydrogenchloride; sodium hydroxide; acetic acid; In tetrahydrofuran; water;

upstream raw materials:

2-chloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3H)-yl)benzeneacetonitrile

chloroform

Downstream raw materials:

2-[3,5-dichloro-4-(4-chlorobenzyl)phenyl]-1,2,4-triazine-3,5(2H,4H)-dione

2,6-dichloro-α-(4-chlorophenyl)-4-(4,5-dihydro-3,5-dioxo-1,2,4-triazin-2(3 H)-yl)benzeneacetic acid

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