tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate)

Base Information

Chemical Name:tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate)
CAS No.:894094-34-9
Molecular Formula:C₂₃H₃₄O₇P₂
Molecular Weight:484.466
Hs Code.:

Synonyms:tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate)

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Chemical Property of tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate)

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Technology Process of tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate)

There total 1 articles about tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1,3-bis(bromomethyl)-5-benzyloxybenzene

: 122-52-1
triethyl phosphite

: 894094-34-9
tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate)

Guidance literature:: at 160 ℃; for 3h;
DOI:10.1055/s-2006-926401

Reference yield: 92.0%

: 894094-34-9
tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate)

: 104-87-0
4-methyl-benzaldehyde

: 894094-36-1
1-Benzyloxy-3,5-bis-((E)-2-p-tolyl-vinyl)-benzene

Guidance literature:: tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate); With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

4-methyl-benzaldehyde; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1055/s-2006-926401

Reference yield: 88.0%

: 894094-34-9
tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate)

: 123-11-5
4-methoxy-benzaldehyde

: 894094-35-0
1-Benzyloxy-3,5-bis-[(E)-2-(4-methoxy-phenyl)-vinyl]-benzene

Guidance literature:: tetraethyl [[5-(benzyloxy)-1,3-phenylene]di(methylene)]bis(phosphonate); With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

4-methoxy-benzaldehyde; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1055/s-2006-926401