N-(2-nitrophenylsulfonyl)-2-benzylsulfanyl-1,4,5,6-tetrahydropyrimidine

Base Information

Chemical Name:N-(2-nitrophenylsulfonyl)-2-benzylsulfanyl-1,4,5,6-tetrahydropyrimidine
CAS No.:135276-88-9
Molecular Formula:C₁₇H₁₇N₃O₄S₂
Molecular Weight:391.472
Hs Code.:

Synonyms:N-(2-nitrophenylsulfonyl)-2-benzylsulfanyl-1,4,5,6-tetrahydropyrimidine

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Chemical Property of N-(2-nitrophenylsulfonyl)-2-benzylsulfanyl-1,4,5,6-tetrahydropyrimidine

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Technology Process of N-(2-nitrophenylsulfonyl)-2-benzylsulfanyl-1,4,5,6-tetrahydropyrimidine

There total 4 articles about N-(2-nitrophenylsulfonyl)-2-benzylsulfanyl-1,4,5,6-tetrahydropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 135276-86-7
2-benzylthio-1,4,5,6-tetrahydropyrimidine hydrobromide

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 135276-88-9
N-(2-nitrophenylsulfonyl)-2-benzylsulfanyl-1,4,5,6-tetrahydropyrimidine

Guidance literature:: With triethylamine; In dichloromethane; for 1h; Ambient temperature;
DOI:10.3987/COM-92-6285

Reference yield: 91.0%

: C₁₁H₁₄N₂S*HI

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 135276-88-9
N-(2-nitrophenylsulfonyl)-2-benzylsulfanyl-1,4,5,6-tetrahydropyrimidine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/acs.jmedchem.6b00847

Reference yield:

: 100-39-0
benzyl bromide

: 135276-88-9
N-(2-nitrophenylsulfonyl)-2-benzylsulfanyl-1,4,5,6-tetrahydropyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / Heating

2: NEt₃ / CH₂Cl₂ / Ambient temperature

With triethylamine; In methanol; dichloromethane;
DOI:10.1016/0040-4039(91)80654-O