(S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene

Base Information

Chemical Name:(S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene
CAS No.:1034015-93-4
Molecular Formula:C₂₆H₂₄N₂O₂
Molecular Weight:396.489
Hs Code.:

Synonyms:(S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene

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Technology Process of (S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene

There total 1 articles about (S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20989-17-7
(2S)-2-phenylglycinol

: 4436-04-8
4,6-dimethylisophthaloyl dichloride

: 1034015-93-4
(S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene

Guidance literature:: (2S)-2-phenylglycinol; 4,6-dimethylisophthaloyl dichloride; With triethylamine; In tetrahydrofuran; at 20 ℃; for 3h;

With methanesulfonyl chloride; In tetrahydrofuran; at 20 ℃; for 15h; Further stages.;
DOI:10.1039/b800387d

Reference yield: 57.0%

: 1034015-93-4
(S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene

: ruthenium(III) chloride trihydrate

: 123-54-6,81235-32-7
acetylacetone

: C₃₂H₃₀N₂O₅Ru

Guidance literature:: (S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene; ruthenium(III) chloride trihydrate; With cyclo-octa-1,5-diene; zinc; In ethanol; at 80 ℃; for 24h; Inert atmosphere; Schlenk technique;

acetylacetone; In ethanol; at 20 ℃; for 20h; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.202100837

Reference yield: 45.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 1034015-93-4
(S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene

: 123-54-6,81235-32-7
acetylacetone

: 7440-66-6
zinc

: mer-[(S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene^(1-)]Ru(CO)(acetylacetonate)

Guidance literature:: With 1,5-cyclooctadiene; In ethanol; under Ar; EtOH and 1,5-cyclooctadiene added to mixt. of RuCl3*3H2O, bisoxazolinyl compd. and Zn, mixt. refluxed for 24 h, cooled, acetylacetone added, stirred at room temp. for 20 h; evapd. under vac., residue extd. with toluene, extract concd., column chromy. (silica gel, EtOAc/hexane 1/5); elem. anal.;
DOI:10.1021/om800953f